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Their characteristic dimensions are in 50\u20131000\u00a0nm scale, typically assembled from a variety of bioorganic \u201cbuilding blocks\u201d. Among the various functions that these mesoscale compartments carry out, protection of the content from the environment is central. Finding synthetic pathways to similarly complex and functional particles from technologically friendly inorganic nanoparticles (NPs) is needed for a multitude of biomedical, biochemical, and biotechnological processes. Here, it is shown that FeS\n                    <jats:sub>2<\/jats:sub>\n                    NPs stabilized by\n                    <jats:sc>l<\/jats:sc>\n                    \u2010cysteine self\u2010assemble into multicompartment supraparticles (mSPs). The NPs initially produce \u224855\u00a0nm concave assemblies that reconfigure into \u224875\u00a0nm closed mSPs with \u2248340 interconnected compartments with an average size of \u22485\u00a0nm. The intercompartmental partitions and mSP surface are formed primarily from FeS\n                    <jats:sub>2<\/jats:sub>\n                    and Fe\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>3<\/jats:sub>\n                    NPs, respectively. The intermediate formation of cup\u2010like particles enables encapsulation of biological cargo. This capability is demonstrated by loading mSPs with DNA and subsequent transfection of mammalian cells. Also it is found\u00a0that the temperature stability of the DNA cargo is enhanced compared to the traditional delivery vehicles. These findings demonstrate that biomimetic compartmentalized particles can be used to successfully encapsulate and enhance temperature stability of the nucleic acid cargo for a variety of bioapplications.\n                  <\/jats:p>","DOI":"10.1002\/adma.202211244","type":"journal-article","created":{"date-parts":[[2023,3,25]],"date-time":"2023-03-25T16:07:40Z","timestamp":1679760460000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":10,"title":["Self\u2010Organization of Iron Sulfide Nanoparticles into Complex Multicompartment Supraparticles"],"prefix":"10.1002","volume":"35","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-8166-0892","authenticated-orcid":false,"given":"E. 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