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The open hydrophilic channels, large periods, and robust physical properties of PCs are advantageous to many host\u2013guest interactions and yet not fully exploited, especially in the fields of functional nanomaterials. Here, the self\u2010assembly of poly(ethylene oxide)\u2010<jats:italic>block<\/jats:italic>\u2010polystyrene block copolymers is systematically investigated and a series of robust PCs is developed via a cosolvent method. Ordered nanoporous metal oxide particles are obtained by selectively filling the hydrophilic channels of PCs via an impregnation strategy, followed by a two\u2010step thermal treatment. Based on this versatile PC platform, the general synthesis of a library of ordered porous particles with different pore structures  , tunable large pore size (18\u201378\u00a0nm), high specific surface areas (up to 123.3\u00a0m<jats:sup>2<\/jats:sup>\u00a0g<jats:sup>\u22121<\/jats:sup> for WO<jats:sub>3<\/jats:sub>) and diverse framework compositions, such as transition and non\u2010transition metal oxides, rare earth chloride oxides, perovskite, pyrochlore, and high\u2010entropy metal oxides is demonstrated. As typical materials obtained via this method, ordered porous WO<jats:sub>3<\/jats:sub> particles have the advantages of open continuous structure and semiconducting properties, thus showing superior gas sensing performances toward hydrogen sulfide.<\/jats:p>","DOI":"10.1002\/adma.202313920","type":"journal-article","created":{"date-parts":[[2024,4,18]],"date-time":"2024-04-18T06:14:35Z","timestamp":1713420875000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":35,"title":["A Versatile Synthesis Platform Based on Polymer Cubosomes for a Library of Highly Ordered Nanoporous Metal Oxides Particles"],"prefix":"10.1002","volume":"36","author":[{"given":"Wenhe","family":"Xie","sequence":"first","affiliation":[{"name":"Department of Chemistry Shanghai Stomatological Hospital &amp; School of Stomatology State Key Laboratory of Molecular Engineering of Polymers Shanghai Key Laboratory of Molecular Catalysis and Innovative Materials Collaborative Innovation Center of Chemistry for Energy Material (iChEM) Fudan University  Shanghai 200433 China"},{"name":"State Key Lab of Transducer Technology, Shanghai Institute of Microsystem and Information Technology Chinese Academy of Sciences  Shanghai 200050 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xinyu","family":"Huang","sequence":"additional","affiliation":[{"name":"Department of Chemistry Shanghai Stomatological Hospital &amp; 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