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However, achieving reversible switching between extreme sticky and slippery states remains a formidable challenge due to the opposing requirements for energy dissipation on gel surfaces. Herein, a self\u2010adaptive bicontinuous fluorogel is introduced that decouples lubrication and adhesion at varying temperatures. The phase\u2010separated fluorogel comprises a soft fluorinated lubricating phase and a stiff yet thermal\u2010responsive load\u2010bearing phase. At ambient temperature, the fluorogel exhibits a highly slippery surface owing to a low\u2010energy\u2010dissipating lubricating layer, demonstrating an ultralow friction coefficient of 0.004. Upon heating, the fluorogel transitions into a highly dissipating state via hydrogen bond dissociation, concurrently releasing adhesive dangling chains to make the surface highly sticky with an adhesion strength of \u2248362\u00a0kPa. This approach provides a promising foundation for creating advanced adaptive materials with on\u2010demand self\u2010adhesive and self\u2010lubricating capabilities.<\/jats:p>","DOI":"10.1002\/adma.202411273","type":"journal-article","created":{"date-parts":[[2024,10,14]],"date-time":"2024-10-14T10:20:08Z","timestamp":1728901208000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":61,"title":["Making Sticky\u2010Slippery Switchable Fluorogels Through Self\u2010Adaptive Bicontinuous Phase Separation"],"prefix":"10.1002","volume":"36","author":[{"given":"Xiaoxia","family":"Li","sequence":"first","affiliation":[{"name":"State Key Laboratory for Modification of Chemical Fibers and Polymer Materials College of Chemistry and Chemical Engineering &amp; Center for Advanced Low\u2010dimension Materials Donghua University  2999 North Renmin Road Shanghai 201620 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