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Downsizing catalysts to single\u2010atom catalysts (SACs), dual\u2010atom catalysts (DACs), and sub\u2010nanocluster catalysts (SNCCs) has generated highly active and selective CO\n                    <jats:sub>2<\/jats:sub>\n                    transformation into highly reduced products. This is\u00a0due to the introduction of numerous active sites, highly unsaturated coordination environments, efficient atom utilization, and confinement effect compared to their nanoparticle counterparts. Herein, recent Cu\u2010based SACs are first reviewed and the newly emerged DACs and SNCCs expanding the catalysis of SACs to electrocatalytic CO\n                    <jats:sub>2<\/jats:sub>\n                    reduction (CO\n                    <jats:sub>2<\/jats:sub>\n                    RR) to high\u2010value products are discussed. Tandem Cu\u2010based SAC\u2013nanocatalysts (NCs) (SAC\u2013NCs) are also discussed for the CO\n                    <jats:sub>2<\/jats:sub>\n                    RR to high\u2010value products. Then, the non\u2010Cu\u2010based SACs, DACs, SAC\u2013NCs, and SNCCs and theoretical calculations of various transition\u2010metal catalysts for CO\n                    <jats:sub>2<\/jats:sub>\n                    RR to high\u2010value products are summarized. Compared to previous achievements of less\u2010reduced products, this review focuses on the double objective of achieving full CO\n                    <jats:sub>2<\/jats:sub>\n                    reduction and increasing the selectivity and formation rate toward C\u2013C coupled products with additional emphasis on the stability of the catalysts. Finally, through combined theoretical and experimental research, future outlooks are offered to further develop the CO\n                    <jats:sub>2<\/jats:sub>\n                    RR into high\u2010value products over isolated atoms and sub\u2010nanometal clusters.\n                  <\/jats:p>","DOI":"10.1002\/adma.202414169","type":"journal-article","created":{"date-parts":[[2024,11,27]],"date-time":"2024-11-27T00:36:31Z","timestamp":1732667791000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":113,"title":["Experimental and Theoretical Insights into Single Atoms, Dual Atoms, and Sub\u2010Nanocluster Catalysts for Electrochemical CO\n                    <sub>2<\/sub>\n                    Reduction (CO\n                    <sub>2<\/sub>\n                    RR) to High\u2010Value Products"],"prefix":"10.1002","volume":"36","author":[{"given":"Abebe Reda","family":"Woldu","sequence":"first","affiliation":[{"name":"Department of Chemistry and Key Laboratory for Preparation and Application of Ordered Structural Materials of Guangdong Province Shantou University  Guangdong 515063 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Asfaw G.","family":"Yohannes","sequence":"additional","affiliation":[{"name":"Department of Chemistry University of Calgary 2500 University Drive NW  Calgary Alberta T2N 1N4 Canada"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zanling","family":"Huang","sequence":"additional","affiliation":[{"name":"Department of Chemistry and Key Laboratory for Preparation and Application of Ordered Structural Materials of Guangdong Province Shantou University  Guangdong 515063 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Pierre","family":"Kennepohl","sequence":"additional","affiliation":[{"name":"Department of Chemistry University of Calgary 2500 University Drive NW  Calgary Alberta T2N 1N4 Canada"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-2258-3126","authenticated-orcid":false,"given":"Didier","family":"Astruc","sequence":"additional","affiliation":[{"name":"ISM, UMR CNRS 5255 University of Bordeaux  Talence Cedex 33405 France"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Liangsheng","family":"Hu","sequence":"additional","affiliation":[{"name":"Department of Chemistry and Key Laboratory for Preparation and Application of Ordered Structural Materials of Guangdong Province Shantou University  Guangdong 515063 P. R. China"},{"name":"Chemistry and Chemical Engineering Guangdong Laboratory  Shantou 515063 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiao\u2010Chun","family":"Huang","sequence":"additional","affiliation":[{"name":"Department of Chemistry and Key Laboratory for Preparation and Application of Ordered Structural Materials of Guangdong Province Shantou University  Guangdong 515063 P. R. China"},{"name":"Chemistry and Chemical Engineering Guangdong Laboratory  Shantou 515063 P. R. 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