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Unfortunately, their structures are prone to aggregation and stacking, hindering further shuttle of lithium ions and electrons, resulting in lower discharge capacity. Therefore, the introduction of interlayer spacers for the preparation of MXene\u2010based hybrids has attracted much attention. Introducing Prubssian blue analogues (PBAs) as a new interlayer spacer to combine with MXene nanosheets can not only preserve the high conductivity of MXene and inhibit the volume expansion and structural degradation of the PBA component, but also inherit the characteristics of large specific surface area and high porosity of PBAs. By intelligent regulating the size of MXene sheets, Co\u2010PBA@MXene hybrids with common sandwich\u2010like structures and superior core\u2010shell\u2010like structures have been successfully obtained. Furthermore, Co@M(<jats:italic>x<\/jats:italic>:<jats:italic>y<\/jats:italic>) hybrids are prepared by intelligently adjusting the shell thickness of MXene through intelligently controlling of the mass ratio between Co\u2010PBA and MXene. Among them, the Co@M(5:2) anode exhibits an excellent capacity (603\u00a0mA h g<jats:sup>\u22121<\/jats:sup> at 0.2 A g<jats:sup>\u22121<\/jats:sup> after 100 cycles) and superior long\u2010term cycling stability due to the protective and conductive properties provided by the MXene shell and multi\u2010redox pairs and rich porosity from Co\u2010PBA core.<\/jats:p>","DOI":"10.1002\/adma.202416665","type":"journal-article","created":{"date-parts":[[2025,1,10]],"date-time":"2025-01-10T05:08:16Z","timestamp":1736485696000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":81,"title":["Prussian Blue Analogues \u201cDressed\u201d in MXene Nanosheets Tightly for High Performance Lithium\u2010Ion Batteries"],"prefix":"10.1002","volume":"37","author":[{"given":"Yuxin","family":"Shi","sequence":"first","affiliation":[{"name":"School of Chemistry and Chemical Engineering Yangzhou University  Yangzhou Jiangsu 225002 P. R. 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