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This review critically examines\u00a0the limitations of these traditional approaches and emphasize the need of systematic experimental designs that independently vary structural parameters, along with advanced analytical methods capable of resolving active\u2010site ambiguity, are critically reviewed. Recent developments employing orthogonal material libraries, rigorous experimental controls, catalyst passport metadata, and advanced multivariate and meta\u2010analytical tools have emerged as robust frameworks for bias\u2010resistant catalyst design. 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