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Herein, defect\u2010rich trimetallic AuCuRh nanowires (AuCuRh NWs) with a large number of grain boundaries, twin boundaries, and atomic steps are successfully synthesized by galvanic replacement reaction. Due to its self\u2010stability and high activity, AuCuRh NWs can efficiently drive the stable NO\n                    <jats:sub>2<\/jats:sub>\n                    RR at 0\u00a0V potential (Faradaic efficiency: 98.32%, NH\n                    <jats:sub>3<\/jats:sub>\n                    yield rate: 20.49\u00a0mg h\n                    <jats:sup>\u22121<\/jats:sup>\n                    mg\n                    <jats:sub>cat<\/jats:sub>\n                    <jats:sup>\u22121<\/jats:sup>\n                    ). Moreover, AuCuRh NWs also reveal excellent electrocatalytic activity for the formaldehyde electrooxidation reaction (FOR), which can reach 10\u00a0mA cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    at only 0.35\u00a0V potential. The NO\n                    <jats:sub>2<\/jats:sub>\n                    RR||FOR electrolysis system assembled with AuCuRh NWs requires only the electrolysis voltage of 0.38\u00a0V to achieve the co\u2010production of NH\n                    <jats:sub>3<\/jats:sub>\n                    , formate, and hydrogen and ultra\u2010stable continuous electrolysis for 300\u00a0hours. The NO\n                    <jats:sub>2<\/jats:sub>\n                    RR||FOR electrolysis system can be further decreased to only 0.29\u00a0V under illumination due to plasmon\u2010enhanced activity. This study provides an energy\u2010efficient coupling strategy for the stable co\u2010production of value\u2010added chemicals.\n                  <\/jats:p>","DOI":"10.1002\/adma.202513320","type":"journal-article","created":{"date-parts":[[2025,10,8]],"date-time":"2025-10-08T08:33:08Z","timestamp":1759912388000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":10,"title":["Low\u2010Voltage Driven Co\u2010Production of Ammonia, Formate, and Hydrogen From Nitrite Reduction Coupled Formaldehyde Oxidation System on Ultra\u2010Stable AuCuRh Nanowires under Illumination"],"prefix":"10.1002","volume":"38","author":[{"given":"Ze\u2010Nong","family":"Zhang","sequence":"first","affiliation":[{"name":"Key Laboratory of Macromolecular Science of Shaanxi Province School of Chemistry and Chemical Engineering Shaanxi Normal University  Xi'an 710062 P. R. 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