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In even lower symmetry materials, such as monoclinic \u2010Ga\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>3<\/jats:sub>\n                    (bGO), hyperbolic shear polaritons (HShPs) further enhance the directionality. Yet, HShPs are intrinsically supported only within narrow frequency ranges defined by the phonon frequencies of the host material. Here, we report spectral tuning of HShPs in bGO by isotopic substitution. Employing near\u2010field optical microscopy to image HShPs in\n                    <jats:sup>18<\/jats:sup>\n                    O bGO films homoepitaxially grown on a\n                    <jats:sup>16<\/jats:sup>\n                    O bGO substrate, we demonstrate a spectral redshift of 40\u00a0cm\n                    <jats:sup>\u22121<\/jats:sup>\n                    for the\n                    <jats:sup>18<\/jats:sup>\n                    O bGO, compared to\n                    <jats:sup>16<\/jats:sup>\n                    O bGO. The technique allows for direct observation and a model\u2010free estimation of the spectral shift driven by isotopic substitution without the need for knowledge of the dielectric tensor. Complementary far\u2010field measurements and ab initio calculations \u2010 in good agreement with the near\u2010field data \u2010 confirm the effectiveness of this estimation. This multifaceted study demonstrates a significant isotopic substitution induced spectral tuning of HShPs into a previously inaccessible frequency range, creating new avenues for technological applications of such highly directional\u00a0polaritons.\n                  <\/jats:p>","DOI":"10.1002\/adma.202514561","type":"journal-article","created":{"date-parts":[[2026,1,10]],"date-time":"2026-01-10T14:05:19Z","timestamp":1768053919000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["Spectral Tuning of Hyperbolic Shear Polaritons in Monoclinic Gallium Oxide via Isotopic Substitution"],"prefix":"10.1002","volume":"38","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-8096-9417","authenticated-orcid":false,"given":"Giulia","family":"Carini","sequence":"first","affiliation":[{"name":"Fritz\u2010Haber\u2010Institut der Max\u2010Planck\u2010Gesellschaft Berlin Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0007-2313-4617","authenticated-orcid":false,"given":"Mohit","family":"Pradhan","sequence":"additional","affiliation":[{"name":"University of Iowa Iowa City USA"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8625-1497","authenticated-orcid":false,"given":"Elena","family":"Gel\u017einyt\u0117","sequence":"additional","affiliation":[{"name":"Fritz\u2010Haber\u2010Institut der Max\u2010Planck\u2010Gesellschaft Berlin Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4987-1873","authenticated-orcid":false,"given":"Andrea","family":"Ardenghi","sequence":"additional","affiliation":[{"name":"Paul\u2010Drude\u2010Institut f\u00fcr Festk\u00f6rperelektronik Leibniz\u2010Institut im Forschungsverbund Berlin e.V. 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