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To overcome this limitation, an electrostatic pre\u2010organization and laser\u2010driven carbonization (EPO\u2013LDC) strategy is developed. Nafion sulfonates electrostatically pre\u2010organize Bi\n                    <jats:sup>3+<\/jats:sup>\n                    at the molecular scale, while ultrafast laser quenching enables non\u2010equilibrium synthesis, initiating simultaneous carbon reconstruction and fluorine\u2010mediated covalent bonding within nanoseconds. This rapid thermal confinement kinetically restricts atomic diffusion, thereby circumventing the aggregation pathways inherent to conventional thermal processes. Concurrently, fluorine ligands offer thermodynamic stabilization through strong Bi\u2500F bonds and optimize charge redistribution via electronegativity\u2010driven orbital hybridization. This dual stabilization achieves a high\u2010density (9.63 wt.%) atomic dispersion of bismuth within a fluorinated porous carbon network (Bi@CF) without aggregation. Theoretical calculations reveal that Bi\u2013F\u2013C sites exhibit an exceptional Li adsorption energy of \u22129.82\u00a0eV, far exceeding those of conventional lithiophilic anodes (\u22121\u2013\u22125\u00a0eV). The combination of atomic\u2010scale lithiophilicity and laser\u2010induced hierarchical porosity enables multiscale ion regulation, resulting in remarkable electrochemical stability. The EPO\u2013LDC strategy thus provides a scalable industrial pathway for producing high\u2010loading single\u2010atom architectures with precisely tailored coordination environments.\n                  <\/jats:p>","DOI":"10.1002\/adma.202517701","type":"journal-article","created":{"date-parts":[[2026,1,16]],"date-time":"2026-01-16T13:22:41Z","timestamp":1768569761000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["Laser\u2010Induced High\u2010Density Bi\u2013F\u2013C Sites to Unleash Potent Li\u207a Adsorption for Stable Lithium Anodes"],"prefix":"10.1002","volume":"38","author":[{"ORCID":"https:\/\/orcid.org\/0009-0009-2546-6783","authenticated-orcid":false,"given":"Chenming","family":"Zhou","sequence":"first","affiliation":[{"name":"Key Laboratory for Anisotropy and Texture of Materials School of Materials Science and Engineering Northeastern University  Shenyang 110819 P. R. 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