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We realize an unprecedented 2D Kondo superlattice, Ta\u2010NbS\n                    <jats:sub>2<\/jats:sub>\n                    , consisting of two coupled metallic 1H\u2010NbS\n                    <jats:sub>2<\/jats:sub>\n                    monolayers intercalated with growth\u2010controlled periodic Ta sublattices. One\u2010step CVD enables tunable periodicities, yielding three Ta\u2010moment motifs: bulk\u2010like simple triangular geometry of  a\u00d7 a (Type I), 2D spin\u2010frustrated 4a\u00d74a (Type II), and 2D saturated  a\u00d7 a (Type III). Beyond the logarithmic resistance upturn at Kondo temperature (\n                    <jats:italic>T<\/jats:italic>\n                    <jats:sub>K<\/jats:sub>\n                    ), we observe anomalous Hall effect evolution from single\u2010impurity to coherent Kondo regimes, reflecting collective Ta\u2010Kondo sublattice interactions. Carrier density modulation tunes the balance between Kondo screening and RKKY interactions, establishing 2D bilayer Ta\u2010NbS\n                    <jats:sub>2<\/jats:sub>\n                    as an ultra\u2010tunable 2D Kondo superlattice for correlated quantum phenomena, with potential applications in spintronics and quantum devices.\n                  <\/jats:p>","DOI":"10.1002\/adma.202520751","type":"journal-article","created":{"date-parts":[[2026,1,16]],"date-time":"2026-01-16T13:26:43Z","timestamp":1768570003000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":2,"title":["Tunable Hetero\u2010Intercalated 2D Superlattice for Frustrated Kondo Triangles"],"prefix":"10.1002","volume":"38","author":[{"given":"Daiyue","family":"Li","sequence":"first","affiliation":[{"name":"State key Laboratory of Quantum Functional Materials Department of Physics and Guangdong Basic Research Center of Excellence for Quantum Science Southern University of Science and Technology (SUSTech)  Shenzhen China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiangyu","family":"Hu","sequence":"additional","affiliation":[{"name":"School of Physics, and State Key Laboratory of Silicon and Advanced Semiconductor Materials Zhejiang University  Hangzhou China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Gang","family":"Wang","sequence":"additional","affiliation":[{"name":"State key Laboratory of Quantum Functional Materials Department of Physics and Guangdong Basic Research Center of Excellence for Quantum Science Southern University of Science and Technology (SUSTech)  Shenzhen China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ruizi","family":"Zhang","sequence":"additional","affiliation":[{"name":"University of Chinese Academy of Sciences and Institute of Physics Chinese Academy of Sciences  Beijing China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xinxi","family":"Liu","sequence":"additional","affiliation":[{"name":"School of Physics, and State Key Laboratory of Silicon and Advanced Semiconductor Materials Zhejiang University  Hangzhou China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Kangdi","family":"Niu","sequence":"additional","affiliation":[{"name":"State key Laboratory of Quantum Functional Materials Department of Physics and Guangdong Basic Research Center of Excellence for Quantum Science Southern University of Science and Technology (SUSTech)  Shenzhen China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zenglong","family":"Guo","sequence":"additional","affiliation":[{"name":"State key Laboratory of Quantum Functional Materials Department of Physics and Guangdong Basic Research Center of Excellence for Quantum Science Southern University of Science and Technology (SUSTech)  Shenzhen China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xizhi","family":"Fu","sequence":"additional","affiliation":[{"name":"Department of Physics Hong Kong University of Science and Technology Clear Water Bay  Hong Kong China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jinbo","family":"Pan","sequence":"additional","affiliation":[{"name":"University of Chinese Academy of Sciences and Institute of Physics Chinese Academy of Sciences  Beijing China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shixuan","family":"Du","sequence":"additional","affiliation":[{"name":"University of Chinese Academy of Sciences and Institute of Physics Chinese Academy of Sciences  Beijing China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Junwei","family":"Liu","sequence":"additional","affiliation":[{"name":"Department of Physics Hong Kong University of Science and Technology Clear Water Bay  Hong Kong 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Devices Southern University of Science and Technology (SUSTech)  Shenzhen 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