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Synthesis consistency is often compromised by incomplete protocols and inconsistent nomenclature, with even well\u2010established MOFs exhibiting substantial variability depending on subtle and frequently unreported factors. To address this critical challenge, we introduce the Material Preparation Information File (MPIF), a modular, machine\u2010 and human\u2010readable format for documenting synthesis protocols alongside key characterization data. Built on the Self\u2010defining Text Archive and Retrieval (STAR) file architecture, MPIF consolidates essential information, including reagents, conditions, equipment, and handling procedures\u2014into a structured format that supports both digital processing and practical laboratory use. To streamline MPIF creation and editing, a web\u2010based interface has been developed (mpif.jackdevans.com). 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