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The process utilizes a deep eutectic solvent composed of calcium chloride, formic acid, and water, which effectively facilitates cellulose dissolution and partial esterification. Followed by dry\u2010jet wet spinning and ethanol\u2010induced coagulation, the initially disordered cellulose chains are reorganized into an ordered, compact fibrillar structure. The resulting fibers showcase a relative crystallinity of 63.9%, tensile strength of 222\u00a0MPa, elongation exceeding 20%, and thermal stability above 180\u00b0C. Furthermore, they possess textile\u2010relevant properties including thermal conductivity of 0.064 W\u00b7m\n                    <jats:sup>\u22121<\/jats:sup>\n                    \u00b7K\n                    <jats:sup>\u22121<\/jats:sup>\n                    , moisture regain of 12.4%, and luster comparable to cuprammonium rayon. Significantly, the process allows for the concurrent recovery of both the solvent and coagulant, maintains fiber reusability, and minimizes waste and costs. The life\u2010cycle assessment indicates that this approach significantly reduces the carbon footprint and resource depletion compared to conventional rayon production. These findings establish a cost\u2010effective, eco\u2010friendly alternative to current solvent systems, addressing both environmental and industrial needs.\n                  <\/jats:p>","DOI":"10.1002\/adma.73389","type":"journal-article","created":{"date-parts":[[2026,5,15]],"date-time":"2026-05-15T15:03:09Z","timestamp":1778857389000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["A Circular Manufacturing Platform for High\u2010Performance Cellulosic Fibers via Hydrogen\u2010Bond Unzipping and Rezipping"],"prefix":"10.1002","volume":"38","author":[{"given":"Zhihan","family":"Tong","sequence":"first","affiliation":[{"name":"State Key Laboratory of Woody Oil Resources Utilization Northeast Forestry University  Harbin Heilongjiang China"},{"name":"College of Chemistry Chemical Engineering and Resource Utilization Northeast Forestry University  Harbin Heilongjiang 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