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Here, an ultra\u2010high\u2010throughput (UHT) combinatorial strategy is introduced for the miniaturized synthesis and screening of polyamine\u2010polyphenolic (\n                    <jats:bold>PaPp<\/jats:bold>\n                    ) coatings (formed in Tris buffer) using droplet microarrays (DMA). Approximately 30\u00a0000\u00a0coatings were generated from binary and ternary combinations of 51 polyphenols (\n                    <jats:bold>Pp<\/jats:bold>\n                    )\u00a0and 12 polyamines (\n                    <jats:bold>Pa<\/jats:bold>\n                    ), each produced in 160\u00a0nL volumes (&lt;5\u00a0mL total reagent use), enabling the rapid identification of hundreds of previously unknown functional materials, including over 225 fluorescent coatings and more than 100 redox\u2010active, metal\u2010reducing surfaces. Antibacterial screening uncovered seven coatings with reproducible activity against\n                    <jats:italic>Pseudomonas aeruginosa<\/jats:italic>\n                    , and subsequent validation on macroscale substrates confirmed up to &lt;1\u2010log colony\u2010forming unit (CFU) reduction against\n                    <jats:italic>P.\u00a0aeruginosa<\/jats:italic>\n                    and\n                    <jats:italic>E. coli<\/jats:italic>\n                    . Importantly, five coatings exhibited multiple functionalities, combining surface stability, intrinsic fluorescence, metal\u2010reducing activity, antibacterial effects, and compatibility with adherent human cells. This UHT approach yields the first comprehensive functionality map of\n                    <jats:bold>PaPp<\/jats:bold>\n                    coatings, revealing previously inaccessible multifunctional materials and demonstrating a scalable strategy for the discovery of surface chemistries with tailored optical, redox, and biological properties.\n                  <\/jats:p>","DOI":"10.1002\/adma.73612","type":"journal-article","created":{"date-parts":[[2026,6,11]],"date-time":"2026-06-11T08:13:01Z","timestamp":1781165581000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Ultra\u2010High\u2010Throughput Discovery of Multifunctional Polyphenolic Coatings on Droplet Microarrays"],"prefix":"10.1002","volume":"38","author":[{"given":"Vania Tanda","family":"Widyaya","sequence":"first","affiliation":[{"name":"Institute of Biological and Chemical Systems\u2010Functional Molecular Systems (IBCS\u2010FMS) Karlsruhe Institute of Technology (KIT)  Eggenstein\u2010Leopoldshafen Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Joaqu\u00edn E. 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