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Herein, we report a hierarchical hydrogel evaporator featuring a thin, porous interfacial photothermal layer composed of fused core\u2013shell carbon\u2010polymer nanospheres, fabricated via interfacial precipitation polymerization. The surface\u2010confined photothermal layer ensures effective thermal confinement and abundant liquid\u2010vapor interfaces, while the underlying hydrogel matrix sustains continuous water replenishment, delivering an exceptional evaporation rate of 6.2\u00a0kg m\n                    <jats:sup>\u22122<\/jats:sup>\n                    h\n                    <jats:sup>\u22121<\/jats:sup>\n                    under one\u2010sun irradiation without requiring bulky 3D architectures. During ZLD operation, direction\u2010dependent transport within the thin porous layer drives lateral advection of concentrated brine away from the active evaporation interface while suppressing through\u2010thickness salt accumulation, thereby enabling localized crystallization in the distal region. As a result, near\u2010complete spatial separation of water evaporation and salt crystallization is achieved from 20 wt.% brine. Outdoor demonstration further delivers 26.6 L m\n                    <jats:sup>\u22122<\/jats:sup>\n                    day\n                    <jats:sup>\u22121<\/jats:sup>\n                    of freshwater and 7.7\u00a0kg m\n                    <jats:sup>\u22122<\/jats:sup>\n                    day\n                    <jats:sup>\u22121<\/jats:sup>\n                    of recovered salt, underscoring the potential of this platform for practical ZLD desalination and mineral recovery.\n                  <\/jats:p>","DOI":"10.1002\/adma.73845","type":"journal-article","created":{"date-parts":[[2026,6,26]],"date-time":"2026-06-26T04:09:54Z","timestamp":1782446994000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["A Porous Interfacial Photothermal Layer of Fused Core\u2013Shell Carbon\u2010Polymer Nanospheres for Directional Salt Crystallization and Zero\u2010Liquid\u2010Discharge"],"prefix":"10.1002","volume":"38","author":[{"given":"Haokun","family":"Shen","sequence":"first","affiliation":[{"name":"School of Chemical Engineering University of New South Wales  Kensington New South Wales Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4761-4670","authenticated-orcid":false,"given":"Shudi","family":"Mao","sequence":"additional","affiliation":[{"name":"Centre For Technology in Water and Wastewater School of Civil and Environmental Engineering University of Technology Sydney  Ultimo New South Wales Australia"},{"name":"School of Chemistry and Materials Science Jiangsu Normal University  Xuzhou Jiangsu China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xin Stella","family":"Zhang","sequence":"additional","affiliation":[{"name":"Centre For Technology in Water and Wastewater School of Civil and Environmental Engineering University of Technology Sydney  Ultimo 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