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Here we report a heteroleptic strategy that exploits steric hindrance effects to precisely modulate the thermodynamic properties of hybrid Cu\n                    <jats:sub>4<\/jats:sub>\n                    I\n                    <jats:sub>4<\/jats:sub>\n                    cluster glass, further enabling ultralong, fracture\u2010free, and perturbation\u2010free TPP\n                    <jats:sub>2<\/jats:sub>\n                    MDP\n                    <jats:sub>2<\/jats:sub>\n                    Cu\n                    <jats:sub>4<\/jats:sub>\n                    I\n                    <jats:sub>4<\/jats:sub>\n                    (TPP\u00a0=\u00a0Triphenylphosphine; MDP\u00a0=\u00a0Methyldiphenylphosphine) glass fibers. The heteroleptic TPP\n                    <jats:sub>2<\/jats:sub>\n                    MDP\n                    <jats:sub>2<\/jats:sub>\n                    Cu\n                    <jats:sub>4<\/jats:sub>\n                    I\n                    <jats:sub>4<\/jats:sub>\n                    core glass not only overcomes the stability limitations of hybrid systems, but also exhibits a notable light yield of 38598 photons MeV\n                    <jats:sup>\u22121<\/jats:sup>\n                    and a low detection limit of 62.2 nGy s\n                    <jats:sup>\u22121<\/jats:sup>\n                    . We assemble these fibers into a flexible scintillation fiber array capable of imaging internal defects in confined spaces. This heteroleptic design principle in cluster glass platform can be extended to other hybrid glass fibers for emerging photonic applications.\n                  <\/jats:p>","DOI":"10.1002\/adma.74844","type":"journal-article","created":{"date-parts":[[2026,8,29]],"date-time":"2026-08-29T04:20:25Z","timestamp":1787977225000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Scintillating Fibers From Stable Heteroleptic Hybrid Glasses for Remote X\u2011Ray Detection"],"prefix":"10.1002","volume":"38","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-6965-6214","authenticated-orcid":false,"given":"Yongsheng","family":"Sun","sequence":"first","affiliation":[{"name":"State Key Laboratory of Luminescent Materials and Devices Guangdong Provincial Key Laboratory of Fibre Laser Materials and Applied Techniques Guangdong Engineering Technology Research and Development Centre of Special Optical Fibre Materials and Devices School of Physics and Optoelectronics South China University of Technology  Guangzhou China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-9723-9832","authenticated-orcid":false,"given":"Shuai","family":"Zhang","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Luminescent Materials and Devices Guangdong Provincial Key Laboratory of Fibre Laser Materials and Applied Techniques Guangdong Engineering Technology Research and Development Centre of Special Optical Fibre Materials and Devices School of Physics and Optoelectronics South China University of Technology  Guangzhou China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yuhan","family":"Liu","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Luminescent Materials and Devices Guangdong Provincial Key Laboratory of Fibre Laser Materials and Applied Techniques Guangdong Engineering Technology Research and Development Centre of Special Optical Fibre Materials and Devices School of Physics and Optoelectronics South China University of Technology  Guangzhou China"},{"name":"School of Materials Science and Engineering South China University of Technology  Guangzhou China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7494-3584","authenticated-orcid":false,"given":"Min","family":"Sun","sequence":"additional","affiliation":[{"name":"Electronic Materials Research Laboratory Key Laboratory of the Ministry of Education International Center for Dielectric Research and State Key Laboratory for Mechanical Behavior of Materials School of Electronic Science and Engineering, Faulty of Electronic and Information Engineering Xi'an Jiaotong University Xi'an China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Kai","family":"Han","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Luminescent Materials and Devices Guangdong Provincial Key Laboratory of Fibre Laser Materials and Applied Techniques Guangdong Engineering Technology Research and Development Centre of Special Optical Fibre Materials and Devices School of Physics and Optoelectronics South China University of Technology  Guangzhou China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0001-3780-4446","authenticated-orcid":false,"given":"Chenliang","family":"Li","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Luminescent Materials and Devices Guangdong Provincial Key Laboratory of Fibre Laser Materials and Applied Techniques Guangdong Engineering Technology Research and Development Centre of Special Optical Fibre Materials and Devices School of Physics and Optoelectronics South China University of Technology  Guangzhou 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