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Nevertheless, achieving ultra\u2010efficient and cost\u2010effective treatment of trace amounts of heavy metals remains a major challenge. Herein, the novel carbon sub\u2010micrometer composites (CSMCs) supported Fe<jats:sup>0<\/jats:sup>@\u03b3\u2010Fe<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub> core\u2010shell clusters nanostructures are designed and synthesized through a series of universally applicable methods. Research data on adsorption behavior clearly revealed that resorcinol\/formaldehyde 1.25\u2010basic ferric acetate (RF\u20101.25BFA) and RF\u20101.25BFA\u2010540 have surprising adsorption capacities. Employing the adsorbent dosage of 0.025\u00a0g\u00a0L<jats:sup>\u22121<\/jats:sup>, the adsorption capacities for 10\u00a0mg\u00a0L<jats:sup>\u22121<\/jats:sup> Cd(II) reached 400.00\u00a0mg\u00a0g<jats:sup>\u22121<\/jats:sup> with ultrafast adsorption kinetics, alongside theoretical maximum adsorption capacities for Cd(II) of 1108.87 and 1065.06\u00a0mg\u00a0g<jats:sup>\u22121<\/jats:sup> using 0.025\u00a0g\u00a0L<jats:sup>\u22121<\/jats:sup> adsorbent, respectively, setting a new record\u2010high level. Additionally, they demonstrated exceptional stability and reusability, maintaining Cd(II) removal efficiency above 95% even after 15 adsorption\u2013desorption cycles. Importantly, this study is the first to unveil a new ultrafast successive two\u2010step enrichment\u2013hydrolysis adsorption mechanism for Cd(II) removal, emphasizing the critical role played by iron clusters nanostructures in constructing a high\u2010alkalinity adsorption microenvironment on the surface of the materials. 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