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The formation of CNPs follows zero\u2010order kinetics with an induction period dependent on the reactivity of the organic precursor. Experimental evidence suggests a surface\u2010catalyzed photochemical process involving a partial change in C\u2010atom hybridization from sp\n                    <jats:sup>2<\/jats:sup>\n                    to sp\n                    <jats:sup>3<\/jats:sup>\n                    , with oxygen\u2010based functional groups passivating the surface of the nanostructures. The presence of additional heteroatoms depends on the structure and composition of the precursor. Contingent on the starting compound, the prepared CNPs can be classified as amorphous carbon nanodots (CNDs) or layered curved\u2010graphene quantum dots (c\u2010GQDs), resembling nano\u2010onion fragments. CNDs are obtained from substituted benzenes or heterocyclic compounds, whereas c\u2010GQDs can be synthesized from benzene. Photophysical characterization of the CNPs shows both wavelength\u2010dependent excitation and emission bands, with constant emission quantum yields in the 1\u201310% range, and wavelength\u2010dependent emission decays displaying several lifetime components in the range 1\u201320\u00a0ns. Triplet exciton lifetimes longer than 5 \u00b5s and wavelength\u2010dependent singlet oxygen production quantum yields in the 10\u201340% range have been measured.\n                  <\/jats:p>","DOI":"10.1002\/advs.202505883","type":"journal-article","created":{"date-parts":[[2025,7,6]],"date-time":"2025-07-06T23:29:44Z","timestamp":1751844584000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Pulsed Laser Synthesis of Carbon Nanostructures from Organic Molecular Liquids: Structure, Kinetics and Photophysical Properties"],"prefix":"10.1002","volume":"12","author":[{"ORCID":"https:\/\/orcid.org\/0009-0004-6506-8038","authenticated-orcid":false,"given":"Antonio","family":"Ribeiro\u2010Gonz\u00e1lez","sequence":"first","affiliation":[{"name":"Department of Organic Chemistry Faculty of Chemical Sciences Universidad Complutense de Madrid  Avenida Complutense s\/n Madrid 28040 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