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However, NO\n                    <jats:sub>x<\/jats:sub>\n                    reduction competes with hydrogen evolution (HER) and can diverge to N\n                    <jats:sub>2<\/jats:sub>\n                    \/N\n                    <jats:sub>2<\/jats:sub>\n                    O, while many catalysts restructure under bias, making results difficult to compare and design rules hard to extract. Cu\u2010MXene hybrids are emerging as a compelling platform because the 2D interface can be engineered to control adsorption, electron (e\n                    <jats:sup>\u2212<\/jats:sup>\n                    ) transfer, and local proton (H\n                    <jats:sup>+<\/jats:sup>\n                    ) activity through Cu speciation (single sites, clusters, oxides, reconstructed surfaces) and MXene terminations\/defects. This critical review summarizes the interfacial control of these catalysts to achieve selective NO\n                    <jats:sub>x<\/jats:sub>\n                    \u2010to\u2010NH\n                    <jats:sub>3<\/jats:sub>\n                    electroconversion. The review provides a comprehensive analysis of intermediates and performance, quantifying using device\u2010relevant metrics (Faradaic efficiency, NH\n                    <jats:sub>3<\/jats:sub>\n                    yield\/partial current, energy efficiency, durability, and selectivity against N\n                    <jats:sub>2<\/jats:sub>\n                    \/N\n                    <jats:sub>2<\/jats:sub>\n                    O and HER). Special emphasis is placed on reactor design, including flow\u2010cell and gas\u2010diffusion electrode (GDE) configurations, which enhance mass transport, stabilize the three\u2010phase boundary, and enable long\u2010term operational stability. Finally, the review emphasizes the use of in situ\/operando methods to investigate the reaction mechanisms, outlines design rules and scale\u2010up priorities for practical NO\n                    <jats:sub>x<\/jats:sub>\n                    upcycling into green ammonia.\n                  <\/jats:p>","DOI":"10.1002\/advs.76280","type":"journal-article","created":{"date-parts":[[2026,6,28]],"date-time":"2026-06-28T12:13:02Z","timestamp":1782648782000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Interfacial Control in Cu\u2013MXene Hybrids Enables Selective NOx\u2010to\u2010NH\n                    <sub>3<\/sub>\n                    Electroconversion: A Critical Review"],"prefix":"10.1002","volume":"13","author":[{"given":"Hafiz Muhammad Adeel","family":"Sharif","sequence":"first","affiliation":[{"name":"Research Center for Eco\u2010Environmental Engineering Dongguan University of Technology Dongguan 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