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The morphology of the photoactive layer plays a critical role in performance improvement of OSCs. Therefore, numerous methods have been developed to optimize the morphology of the photoactive layer and unlock the full potential of the devices. Among them, volatile solid and solvent additives have attracted considerable attention due to their robust enhancement of efficiency and stability, coupled with a simple operational process. Here, the classification and development history of the volatile solid and solvent additives are comprehensively summarized, and the underlying mechanisms of morphology optimization are discussed. Additionally, a summary of volatile additive\u2010induced improvements in interfacial layer performance is provided. Finally, the challenges and prospects for volatile additives are presented.<\/jats:p>","DOI":"10.1002\/advs.77805","type":"journal-article","created":{"date-parts":[[2026,9,17]],"date-time":"2026-09-17T04:54:50Z","timestamp":1789620890000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Volatile Additives Engineering: A Trustworthy Morphology Control Strategy in Non\u2010Fullerene Organic Solar Cells"],"prefix":"10.1002","volume":"13","author":[{"given":"Jianqiang","family":"Qin","sequence":"first","affiliation":[{"name":"College of Materials and Chemistry &amp; Chemical Engineering Chengdu University of Technology  Chengdu P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhiqin","family":"Lai","sequence":"additional","affiliation":[{"name":"College of Materials and Chemistry &amp; Chemical Engineering Chengdu University of Technology  Chengdu P. R. 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