{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,9]],"date-time":"2026-10-09T04:49:03Z","timestamp":1791521343452,"version":"4.3.4"},"reference-count":66,"publisher":"Wiley","license":[{"start":{"date-parts":[[2026,10,8]],"date-time":"2026-10-08T00:00:00Z","timestamp":1791417600000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/creativecommons.org\/licenses\/by\/4.0\/"},{"start":{"date-parts":[[2026,10,8]],"date-time":"2026-10-08T00:00:00Z","timestamp":1791417600000},"content-version":"tdm","delay-in-days":0,"URL":"http:\/\/doi.wiley.com\/10.1002\/tdm_license_1.1"}],"content-domain":{"domain":["advanced.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["Advanced Science"],"abstract":"<jats:title>ABSTRACT<\/jats:title>\n                  <jats:p>\n                    Aqueous Zn\u2010ion batteries (AZIBs) suffer severe degradation at subzero temperatures due to electrolyte freezing, sluggish Zn\n                    <jats:sup>2+<\/jats:sup>\n                    kinetics, and dendrite\u2010induced interfacial instability. Herein, a triple\u2010coupling regulation strategy integrating solvation structure, interfacial chemistry, and crystallographic orientation through a formamide\u2010ethanol deep eutectic electrolyte (ZEFW2) was developed. Molecular dynamics simulations and spectroscopic analyses reveal that ZEFW2 redistributes the primary Zn\n                    <jats:sup>2+<\/jats:sup>\n                    solvation environment, reducing H\n                    <jats:sub>2<\/jats:sub>\n                    O and acetate coordination while introducing formamide coordination and maintaining favorable Zn\n                    <jats:sup>2+<\/jats:sup>\n                    transport. Depth\u2010resolved XPS further reveals a chemically reconstructed Zn interphase containing Zn\u2010O\u2010related inorganic species and persistent N\u2010 and C\u2010containing electrolyte\u2010derived species. The modified solvation and interfacial environments regulate Zn nucleation and promote preferential Zn deposition along the (101) facet, enabling more homogeneous Zn growth and suppressing dendritic morphology. Consequently, Zn||Zn symmetric cells achieve 1400\u00a0h of cycling at \u221220\u00b0C under 1\u00a0mA cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    and 10 mAh cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    , with a Coulombic efficiency of 99.78% over 1200 cycles. Zn||NVO full cells retain 74% of their initial capacity after 1600 cycles at \u221220\u00b0C, while pouch cells demonstrate stable operation at both room and subzero temperatures. This work establishes a molecular\u2010to\u2010interfacial triple\u2010coupling strategy for temperature\u2010resilient AZIBs.\n                  <\/jats:p>","DOI":"10.1002\/advs.78147","type":"journal-article","created":{"date-parts":[[2026,10,9]],"date-time":"2026-10-09T03:54:46Z","timestamp":1791518086000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Triple\u2010Coupling Regulation Enables Dendrite\u2010Free Subzero Aqueous Zn\u2010Ion Batteries"],"prefix":"10.1002","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-2224-1943","authenticated-orcid":false,"given":"Mengyang","family":"Dong","sequence":"first","affiliation":[{"name":"College of Chemistry and Chemical Engineering Hunan Normal University  Changsha China"},{"name":"UQ Dow Centre for Sustainable Engineering Innovation School of Chemical Engineering The University of Queensland  St Lucia Queensland Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhibao","family":"Yang","sequence":"additional","affiliation":[{"name":"College of Chemistry and Chemical Engineering Hunan Normal University  Changsha China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lina","family":"Pan","sequence":"additional","affiliation":[{"name":"College of Chemistry and Chemical Engineering Hunan Normal University  Changsha China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1463-6117","authenticated-orcid":false,"given":"Jie","family":"Qu","sequence":"additional","affiliation":[{"name":"College of Chemistry and Chemical Engineering Hunan Normal University  Changsha China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shangshu","family":"Qian","sequence":"additional","affiliation":[{"name":"College of Chemical and Biological Engineering Zhejiang University  Hangzhou China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jessica","family":"Hamilton","sequence":"additional","affiliation":[{"name":"Australian Synchrotron ANSTO  Clayton VIC Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3027-0816","authenticated-orcid":false,"given":"Bernt","family":"Johannessen","sequence":"additional","affiliation":[{"name":"Australian Synchrotron ANSTO  Clayton VIC Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0004-0802-504X","authenticated-orcid":false,"given":"Yuhui","family":"Tian","sequence":"additional","affiliation":[{"name":"School of Molecular and Life Sciences Curtin University  Bentley Western Australia Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3177-0361","authenticated-orcid":false,"given":"Chao","family":"Xing","sequence":"additional","affiliation":[{"name":"UQ Dow Centre for Sustainable Engineering Innovation School of Chemical Engineering The University of Queensland  St Lucia Queensland Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2026,10,8]]},"reference":[{"key":"e_1_2_8_2_1","doi-asserted-by":"crossref","DOI":"10.1016\/j.est.2024.110849","article-title":"Advances in Zinc\u2010Ion Structural Batteries","volume":"84","author":"Lionetto F.","year":"2024","journal-title":"Journal of Energy Storage"},{"issue":"40","key":"e_1_2_8_3_1","doi-asserted-by":"crossref","first-page":"35237","DOI":"10.1021\/acsnano.5c10278","article-title":"A Systematic Understanding of Zinc Salts in Electrolyte Design for Aqueous Zinc\u2010Ion Batteries","volume":"19","author":"Zhao Q.","year":"2025","journal-title":"ACS Nano"},{"issue":"1","key":"e_1_2_8_4_1","doi-asserted-by":"crossref","DOI":"10.1002\/aenm.202003065","article-title":"Strategies for the Stabilization of Zn Metal Anodes for 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