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In this work we describe the synthesis and characterization of iridium distannylidyne [(Me\n                    <jats:sub>3<\/jats:sub>\n                    P)\n                    <jats:sub>2<\/jats:sub>\n                    Ir(SnAr*)\n                    <jats:sub>2<\/jats:sub>\n                    ][WCA] (\n                    <jats:bold>1a<\/jats:bold>\n                    \/\n                    <jats:bold>1b<\/jats:bold>\n                    ) {[WCA] = [Al(O\n                    <jats:italic>\n                      <jats:sup>t<\/jats:sup>\n                    <\/jats:italic>\n                    Bu\n                    <jats:sup>F<\/jats:sup>\n                    )\n                    <jats:sub>4<\/jats:sub>\n                    ]\n                    <jats:sup>\u2013<\/jats:sup>\n                    (\n                    <jats:bold>1a<\/jats:bold>\n                    ), [BAr\n                    <jats:sup>F<\/jats:sup>\n                    <jats:sub>4<\/jats:sub>\n                    ]\n                    <jats:sup>\u2013<\/jats:sup>\n                    (\n                    <jats:bold>1b<\/jats:bold>\n                    ); Ar* = 2,6\u2010bis(2,4,6\u2010tri\u2010\n                    <jats:italic>iso<\/jats:italic>\n                    \u2010propylphenyl)phenyl,\n                    <jats:italic>\n                      <jats:sup>t<\/jats:sup>\n                    <\/jats:italic>\n                    Bu\n                    <jats:sup>F<\/jats:sup>\n                    = C(CF\n                    <jats:sub>3<\/jats:sub>\n                    )\n                    <jats:sub>3<\/jats:sub>\n                    , Ar\n                    <jats:sup>F<\/jats:sup>\n                    = 3,5\u2010bis(trifluoromethyl)phenyl} as the first transition metal ditetrylidyne.\n                    <jats:bold>1<\/jats:bold>\n                    reacts with two equivalents of CO\n                    <jats:sub>2<\/jats:sub>\n                    to give [(Me\n                    <jats:sub>3<\/jats:sub>\n                    P)\n                    <jats:sub>2<\/jats:sub>\n                    Ir(SnAr*)\n                    <jats:sub>2<\/jats:sub>\n                    (\n                    <jats:italic>\u03bc<\/jats:italic>\n                    <jats:sub>3<\/jats:sub>\n                    \u2010\n                    <jats:italic>\u03b7<\/jats:italic>\n                    <jats:sup>3<\/jats:sup>\n                    \u2010\n                    <jats:italic>\u03ba<\/jats:italic>\n                    <jats:sup>3<\/jats:sup>\n                    \u2010\n                    <jats:italic>O<\/jats:italic>\n                    ,\n                    <jats:italic>C<\/jats:italic>\n                    ,\n                    <jats:italic>O\u2019<\/jats:italic>\n                    \u2010CO\n                    <jats:sub>2<\/jats:sub>\n                    )\n                    <jats:sub>2<\/jats:sub>\n                    ][Al(O\n                    <jats:italic>\n                      <jats:sup>t<\/jats:sup>\n                    <\/jats:italic>\n                    Bu\n                    <jats:sup>F<\/jats:sup>\n                    )\n                    <jats:sub>4<\/jats:sub>\n                    ] (\n                    <jats:bold>2<\/jats:bold>\n                    ). In the presence of excess trimethylphosphine, trimethylsilyl azide reacts with\n                    <jats:bold>1<\/jats:bold>\n                    to form imido\u2010bridged [(Me\n                    <jats:sub>3<\/jats:sub>\n                    P)\n                    <jats:sub>3<\/jats:sub>\n                    Ir(SnAr*)\n                    <jats:sub>2<\/jats:sub>\n                    (\n                    <jats:italic>\u03bc<\/jats:italic>\n                    <jats:sub>2<\/jats:sub>\n                    \u2010N\u2013TMS)][BAr\n                    <jats:sup>F<\/jats:sup>\n                    <jats:sub>4<\/jats:sub>\n                    ]\u00a0 (\n                    <jats:bold>3<\/jats:bold>\n                    ) upon extrusion of N\n                    <jats:sub>2<\/jats:sub>\n                    .\n                  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