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As a demonstration, an oil\u2010soluble supramonomer containing two thiol end groups linked by two ureidopyrimidinone units and a water\u2010soluble monomer bearing two maleimide end groups are employed. Supramolecular interfacial polymerization can be implemented by a thiol\u2013maleimide click reaction at the water\u2013chloroform interface to obtain supramolecular polymeric films. The glass transition temperature of such supramolecular polymers can be well\u2010tuned by simply changing the polymerization time and temperature. It is highly anticipated that this work will provide a facile and general approach to realize control over supramolecular polymerization by transferring the preparation of supramolecular polymers from solutions to water\u2013oil interfaces and construct supramolecular materials with well\u2010defined properties.<\/jats:p>","DOI":"10.1002\/anie.201703572","type":"journal-article","created":{"date-parts":[[2017,5,8]],"date-time":"2017-05-08T06:25:53Z","timestamp":1494224753000},"page":"7639-7643","source":"Crossref","is-referenced-by-count":134,"title":["Supramolecular Interfacial Polymerization: A Controllable Method of Fabricating Supramolecular Polymeric Materials"],"prefix":"10.1002","volume":"56","author":[{"given":"Bo","family":"Qin","sequence":"first","affiliation":[{"name":"Key Lab of Organic Optoelectronics &amp; Molecular Engineering Department of Chemistry Tsinghua University  Beijing 100084 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shuai","family":"Zhang","sequence":"additional","affiliation":[{"name":"Key Lab of Organic Optoelectronics &amp; 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