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Various 1,1,2\u2010triborylalkenes, a class of compounds that have been demonstrated to be potential matrix metalloproteinase (MMP\u20102) inhibitors, were obtained directly in moderate to good yields. The process features mild reaction conditions, a broad substrate scope, and good functional group tolerance. This copper\u2010catalyzed reaction can be conducted on a gram scale to produce the corresponding 1,1,2\u2010triborylalkenes in modest yields. The utility of these products was demonstrated by further transformations of the C\u2212B bonds to prepare\n                    <jats:italic>gem<\/jats:italic>\n                    \u2010dihaloborylalkenes (F, Cl, Br), monohaloborylalkenes (Cl, Br), and\n                    <jats:italic>trans<\/jats:italic>\n                    \u2010diaryldiborylalkenes, which serve as important synthons and have previously been challenging to prepare.\n                  <\/jats:p>","DOI":"10.1002\/anie.201908466","type":"journal-article","created":{"date-parts":[[2019,9,10]],"date-time":"2019-09-10T05:24:31Z","timestamp":1568093071000},"page":"304-309","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":79,"title":["Copper\u2010Catalyzed Triboration of Terminal Alkynes Using B\n                    <sub>2<\/sub>\n                    pin\n                    <sub>2<\/sub>\n                    : Efficient Synthesis of 1,1,2\u2010Triborylalkenes"],"prefix":"10.1002","volume":"59","author":[{"given":"Xiaocui","family":"Liu","sequence":"first","affiliation":[{"name":"Institute of Inorganic Chemistry and Institute for Sustainable Chemistry &amp; Catalysis with Boron Julius-Maximilians-Universit\u00e4t W\u00fcrzburg  Am Hubland 97074 W\u00fcrzburg Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wenbo","family":"Ming","sequence":"additional","affiliation":[{"name":"Institute of Inorganic Chemistry and Institute for Sustainable Chemistry &amp; Catalysis with Boron Julius-Maximilians-Universit\u00e4t W\u00fcrzburg  Am Hubland 97074 W\u00fcrzburg Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-1411-7336","authenticated-orcid":false,"given":"Alexandra","family":"Friedrich","sequence":"additional","affiliation":[{"name":"Institute of Inorganic Chemistry and Institute for Sustainable Chemistry &amp; Catalysis with Boron 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