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However, it remains a great challenge to develop a universal method to prepare 2D mesoporous heterostructures. Herein, we report a composite\u2010micelle\u2010directed interfacial assembly method to synthesize heterostructures of an ultrathin 2D material covered with mesoporous monolayers assembled on both sides. To demonstrate the concept, we first fabricated a new sandwichlike carbon@MXene@carbon mesoporous heterostructure through the self\u2010assembly of exfoliated MXene nanosheets and block copolymer F127\/melamine\u2010formaldehyde resin composite micelles and subsequent thermal treatment. Finally, we demonstrate that the carbon@MXene@carbon mesoporous heterostructured nanosheets manifest remarkably enhanced electrochemical performance as a cathode material for lithium\u2013sulfur batteries.<\/jats:p>","DOI":"10.1002\/anie.202007063","type":"journal-article","created":{"date-parts":[[2020,7,11]],"date-time":"2020-07-11T15:54:15Z","timestamp":1594482855000},"page":"19570-19575","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":91,"title":["Universal Access to Two\u2010Dimensional Mesoporous Heterostructures by Micelle\u2010Directed Interfacial Assembly"],"prefix":"10.1002","volume":"59","author":[{"given":"Jie","family":"Wang","sequence":"first","affiliation":[{"name":"International Research Center for Materials Nanoarchitechtonics (WPI-MANA) National Institute for Materials Science  1-1 Namiki Tsukuba Ibaraki 305-0044 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Unit for Innovative Multiscale Materials Kyushu Institute of Technology  1-1 Sensui-cho, Tobata Kitakyushu Fukuoka 804-8550 Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Miharu","family":"Eguchi","sequence":"additional","affiliation":[{"name":"International Research Center for Materials Nanoarchitechtonics (WPI-MANA) National Institute for Materials Science  1-1 Namiki Tsukuba Ibaraki 305-0044 Japan"},{"name":"School of Chemical Engineering and Australian Institute for, Bioengineering and Nanotechnology (AIBN) The University of Queensland  Brisbane QLD 4072 Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yong\u2010Mook","family":"Kang","sequence":"additional","affiliation":[{"name":"Department of Materials Science and Engineering Korea University  Seoul 02841 Republic of Korea"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jongbeom","family":"Na","sequence":"additional","affiliation":[{"name":"International Research 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