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Control experiments and DFT calculations indicate that both the ortho\u2010F substituents on the polyfluorophenyl boronates and the counterion K\n                    <jats:sup>+<\/jats:sup>\n                    in the carbonate base are critical. The distinguishing features of this procedure include the employment of commercially available starting materials and the broad scope of the reaction with a wide variety of carbonyl compounds giving moderate to excellent yields. Intriguing structural features involving O\u2212H\u22c5\u22c5\u22c5O and O\u2212H\u22c5\u22c5\u22c5N hydrogen bonding, as well as arene\u2010perfluoroarene interactions, in this series of racemic polyfluoroaryl carbinols have also been addressed.\n                  <\/jats:p>","DOI":"10.1002\/anie.202103686","type":"journal-article","created":{"date-parts":[[2021,4,26]],"date-time":"2021-04-26T13:14:58Z","timestamp":1619442898000},"page":"16529-16538","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":24,"title":["Transition Metal Catalyst\u2010Free, Base\u2010Promoted 1,2\u2010Additions of Polyfluorophenylboronates to Aldehydes and Ketones"],"prefix":"10.1002","volume":"60","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-6253-9608","authenticated-orcid":false,"given":"Zhiqiang","family":"Liu","sequence":"first","affiliation":[{"name":"Institute of Inorganic Chemistry and Institute for Sustainable Chemistry &amp; Catalysis with Boron Julius-Maximilians-Universit\u00e4t W\u00fcrzburg  Am Hubland 97074 W\u00fcrzburg Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-1503-0574","authenticated-orcid":false,"given":"Goutam Kumar","family":"Kole","sequence":"additional","affiliation":[{"name":"Institute of Inorganic Chemistry and Institute for Sustainable Chemistry &amp; 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