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Here, we propose a novel strategy for selective extraction of nickel, cobalt, and manganese from spent LiNi\n                    <jats:sub>\n                      <jats:italic>x<\/jats:italic>\n                    <\/jats:sub>\n                    Co\n                    <jats:sub>\n                      <jats:italic>y<\/jats:italic>\n                    <\/jats:sub>\n                    Mn\n                    <jats:sub>\n                      1\u2212\n                      <jats:italic>x<\/jats:italic>\n                      \u2212\n                      <jats:italic>y<\/jats:italic>\n                    <\/jats:sub>\n                    O\n                    <jats:sub>2<\/jats:sub>\n                    (NCM) cathode through the regulation of coordination environment. Depending on adjusting the composition of ligand in transition metal complexes, a tandem leaching and separation system is designed and finally enables nickel, cobalt, and manganese to enrich in the form of NiO, Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    , and Mn\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    with high recovery yields of 99.1\u2009%, 95.1\u2009%, and 95.3\u2009%, respectively. We further confirm that the combination of different transition metals with well\u2010designed ligands is the key to good selectivity. Through our work, fine\u2010tuning the coordination environment of metal ions is proved to have great prospects in the battery recycling industry.\n                  <\/jats:p>","DOI":"10.1002\/anie.202202558","type":"journal-article","created":{"date-parts":[[2022,3,19]],"date-time":"2022-03-19T09:03:57Z","timestamp":1647680637000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":259,"title":["Selective Extraction of Transition Metals from Spent LiNi\n                    <sub>\n                      <i>x<\/i>\n                    <\/sub>\n                    Co\n                    <sub>y<\/sub>\n                    Mn\n                    <sub>\n                      1\u2212\n                      <i>x<\/i>\n                      \u2212\n                      <i>y<\/i>\n                    <\/sub>\n                    O\n                    <sub>2<\/sub>\n                    Cathode via Regulation of Coordination Environment"],"prefix":"10.1002","volume":"61","author":[{"given":"Xin","family":"Chang","sequence":"first","affiliation":[{"name":"CAS Key Laboratory of Molecular Nanostructure and Nanotechnology CAS Research\/Education Centre for Excellence in Molecular Sciences Beijing National Laboratory for Molecular Sciences (BNLMS) Institute of Chemistry Chinese Academy of Sciences  Beijing 100190 P. R. China"},{"name":"University of Chinese Academy of Sciences (UCAS)  Beijing 100049 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Min","family":"Fan","sequence":"additional","affiliation":[{"name":"CAS Key Laboratory of Molecular Nanostructure and Nanotechnology CAS Research\/Education Centre for Excellence in Molecular Sciences Beijing National Laboratory for Molecular Sciences (BNLMS) Institute of Chemistry Chinese Academy of Sciences  Beijing 100190 P. R. China"},{"name":"University of Chinese Academy of Sciences (UCAS)  Beijing 100049 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chao\u2010Fan","family":"Gu","sequence":"additional","affiliation":[{"name":"CAS Key Laboratory of Molecular Nanostructure and Nanotechnology CAS Research\/Education Centre for Excellence in Molecular Sciences Beijing National Laboratory for Molecular Sciences (BNLMS) Institute of Chemistry Chinese Academy of Sciences  Beijing 100190 P. R. China"},{"name":"University of Chinese Academy of Sciences (UCAS)  Beijing 100049 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wei\u2010Huan","family":"He","sequence":"additional","affiliation":[{"name":"CAS Key Laboratory of Molecular Nanostructure and Nanotechnology CAS Research\/Education Centre for Excellence in Molecular Sciences Beijing National Laboratory for Molecular Sciences (BNLMS) Institute of Chemistry Chinese Academy of Sciences  Beijing 100190 P. R. China"},{"name":"University of Chinese Academy of Sciences (UCAS)  Beijing 100049 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qinghai","family":"Meng","sequence":"additional","affiliation":[{"name":"CAS Key Laboratory of Molecular Nanostructure and Nanotechnology CAS Research\/Education Centre for Excellence in Molecular Sciences Beijing National Laboratory for Molecular Sciences (BNLMS) Institute of Chemistry Chinese Academy of Sciences  Beijing 100190 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Li\u2010Jun","family":"Wan","sequence":"additional","affiliation":[{"name":"CAS Key Laboratory of Molecular Nanostructure and Nanotechnology CAS Research\/Education Centre for Excellence in Molecular Sciences Beijing National Laboratory for Molecular Sciences (BNLMS) Institute of Chemistry Chinese Academy of Sciences  Beijing 100190 P. R. China"},{"name":"University of Chinese Academy of Sciences (UCAS)  Beijing 100049 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-0322-8476","authenticated-orcid":false,"given":"Yu\u2010Guo","family":"Guo","sequence":"additional","affiliation":[{"name":"CAS Key Laboratory of Molecular Nanostructure and Nanotechnology CAS Research\/Education Centre for Excellence in Molecular Sciences Beijing National Laboratory for Molecular Sciences (BNLMS) Institute of Chemistry Chinese Academy of Sciences  Beijing 100190 P. R. 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