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Owing to the structural tension and electron\u2010donating properties of the nitrogen atoms in the macrocycle, reaction selectively proceeds between the adjacent benzene rings outside the macrocycle. C\u2010BN shows a highly centrosymmetric structure with two multiple resonance (MR) fragments bridged by tertiary amine groups at the 1,3 positions of the benzene ring. Benefiting from the large intermolecular distance (&gt;4.6\u2005\u00c5) between adjacent MR\u2010emitting cores, C\u2010BN also exhibits excellent narrowband emitting features against aggregation\u2010induced quenching and spectrum broadening. Optimized organic light\u2010emitting diode devices based on C\u2010BN exhibit high maximum external quantum efficiencies of 24.7\u201326.6\u2009% and small full width at half maximums of 25\u201328\u2005nm over a wide doping range of 1\u201312\u2005wt\u2009%.<\/jats:p>","DOI":"10.1002\/anie.202213585","type":"journal-article","created":{"date-parts":[[2022,10,25]],"date-time":"2022-10-25T05:24:35Z","timestamp":1666675475000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":72,"title":["One\u2010Shot Synthesis of B\/N\u2010Doped Calix[4]arene Exhibiting Narrowband Multiple Resonance Fluorescence"],"prefix":"10.1002","volume":"61","author":[{"given":"Tianjiao","family":"Fan","sequence":"first","affiliation":[{"name":"Key Lab of Organic Optoelectronics and Molecular Engineering of Ministry of Education Department of Chemistry Tsinghua University  Beijing 100084 P. R. 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