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Here, for the first time, we employed the McMurry coupling reaction to prepare \u03c0\u2010conjugated anion exchange membranes (AEMs). The inter\u2010chain \u03c0\u2010\u03c0 stacking between adjacent benzene rings induces directional self\u2010assembly aggregation and enables highly ordered ion\u2010conductive channels. The resulting structure was characterized through UV\/VIS spectrum, X\u2010ray diffraction (XRD) pattern, small\u2010angle X\u2010ray scattering (SAXS), transmission electron microscopy (TEM) and density functional theory (DFT) calculations, leading to high OH\n                    <jats:sup>\u2212<\/jats:sup>\n                    conductivity of 135.5\u2005mS\u2009cm\n                    <jats:sup>\u22121<\/jats:sup>\n                    at 80\u2009\u00b0C. Furthermore, the double bonds in the \u03c0\u2010conjugated system also trigger in situ self\u2010crosslinking of the AEMs to enhance dimensional and alkaline stability. Benefiting from this advantage, the as\u2010obtained Cr\u2010QPPV\u20102.51 AEM exhibits superior alkaline stability (95\u2009% conductivity retention after 3000\u2005hrs in 1\u2005M KOH at 80\u2009\u00b0C) and high mechanical strength of 34.8\u2005MPa. Moreover, the fuel cell using Cr\u2010QPPV\u20102.51 shows a maximum peak power density of 1.27\u2005W\u2009cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    at 80\u2009\u00b0C.\n                  <\/jats:p>","DOI":"10.1002\/anie.202215017","type":"journal-article","created":{"date-parts":[[2022,11,24]],"date-time":"2022-11-24T22:50:50Z","timestamp":1669330250000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":52,"title":["A \u03c0\u2010Conjugated Anion\u2010Exchange Membrane with an Ordered Ion\u2010Conducting Channel via the McMurray Coupling Reaction"],"prefix":"10.1002","volume":"62","author":[{"given":"Fan","family":"Zhang","sequence":"first","affiliation":[{"name":"Anhui Engineering Laboratory of Functional Membrane Materials and Technology Collaborative Innovation Centre of Chemistry for Energy Materials School of Chemistry and Material Science University of Science and Technology of China  Hefei 230026 P. 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