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The transformation proceeds through sequential intermolecular and intramolecular Friedel\u2013Crafts\u2010type processes under acidic conditions, enabling one\u2010pot construction of fused benzofuran frameworks. The method shows good substrate scope, providing products in moderate yields and demonstrating gram\u2010scale practicality. Based on this scaffold, two donor units are developed and incorporated into multi\u2010resonance thermally activated delayed fluorescence (MR\u2010TADF) emitters, namely BNFFA and BNFFC. Both compounds exhibit narrowband emission (full with at half maximum = 20 and 25 nm) and decent delayed fluorescence. Organic light\u2010emitting diodes based on these emitters achieved maximum external quantum efficiencies of 23.5% and 29.3%, with blue\u2010cyan emissions suitable for emerging four\u2010primary wide\u2010color\u2010gamut displays.<\/jats:p>","DOI":"10.1002\/anie.2320378","type":"journal-article","created":{"date-parts":[[2026,9,29]],"date-time":"2026-09-29T04:04:04Z","timestamp":1790654644000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Metal\u2010Free One\u2010Pot Access to Benzofuran Building Blocks Toward Efficient Narrowband Blue\u2013Cyan Emitters"],"prefix":"10.1002","author":[{"given":"Guopeng","family":"Huang","sequence":"first","affiliation":[{"name":"Shenzhen Key Laboratory of New Information Display and Storage Materials, College of Materials Science and Engineering Shenzhen University  Shenzhen P. R. 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