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Here, we develop an In\u2013Bi catalyst by incorporating oxophilic indium (In) into a bismuth (Bi) matrix. During the co\u2010reduction of oxalic acid and NO\n                    <jats:sub>3<\/jats:sub>\n                    <jats:sup>\u2212<\/jats:sup>\n                    , the In\u2013Bi catalyst delivers an exceptional Faradaic efficiency toward glycine (FE\n                    <jats:sub>Glycine<\/jats:sub>\n                    ) of 83.3% with an industrial\u2010level current density of 361.3\u00a0mA cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    , together with a glycine production rate of 4.3\u00a0mol h\n                    <jats:sup>\u22121<\/jats:sup>\n                    g\n                    <jats:sub>cat.<\/jats:sub>\n                    <jats:sup>\u22121<\/jats:sup>\n                    . It outperforms pristine Bi and previously reported state\u2010of\u2010the\u2010art catalysts. Large\u2010scale glycine electrosynthesis is further demonstrated over a 10 cm\n                    <jats:sup>2<\/jats:sup>\n                    In\u2013Bi electrode, achieving a total current of 1.5 A with FE\n                    <jats:sub>Glycine<\/jats:sub>\n                    of 68.5% and yielding 1.4\u00a0g of glycine in 6 h. Mechanistically, oxalic acid and NO\n                    <jats:sub>3<\/jats:sub>\n                    <jats:sup>\u2212<\/jats:sup>\n                    first form glyoxylic acid oxime (GAO). Subsequently, In sites act as an \u201cactive hydrogen pump\u201d to accelerate H\n                    <jats:sub>2<\/jats:sub>\n                    O dissociation, providing abundant surface\u2010active hydrogen (*H) for efficient GAO hydrogenation to glycine. Meanwhile, the incorporation of In modulates the electronic structure of the Bi matrix, enhancing GAO adsorption and electron transfer. The synergistic regulation of *H supply and electronic structure accelerates the conversion of GAO to glycine, resulting in superior performance of In\u2013Bi.\n                  <\/jats:p>","DOI":"10.1002\/anie.2390339","type":"journal-article","created":{"date-parts":[[2026,10,10]],"date-time":"2026-10-10T03:53:38Z","timestamp":1791604418000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Enhanced Electrochemical C\u2013N Coupling for Glycine Synthesis via an Active Hydrogen Pump"],"prefix":"10.1002","author":[{"given":"Jiankang","family":"Liu","sequence":"first","affiliation":[{"name":"Institute of Rare and Scattered Elements College of Chemistry Liaoning University  Shenyang P. R. China"},{"name":"Beijing Synchrotron Radiation Facility Institute of High Energy Physics Chinese Academy of Sciences  Beijing P. R. 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