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In this study, we report the successful isolation of a stannabismuthene (\n                    <jats:bold>2<\/jats:bold>\n                    ), a Sn\/Bi analog of imines, achieved through the kinetic stabilization provided by a bulky terphenyl substituent. The stannabismuthene was synthesized via a one\u2010pot reduction of BiBr\n                    <jats:sub>3<\/jats:sub>\n                    and carboranyl distannene (\n                    <jats:bold>1<\/jats:bold>\n                    ) using two equivalents of KC\n                    <jats:sub>8<\/jats:sub>\n                    in THF, and it has been unambiguously characterized through spectroscopic analysis, x\u2010ray diffraction, and DFT calculations. This compound features a Sn\u2550Bi double bond, which acts as a \u03c0 donor, coordinating with AgNTf\n                    <jats:sub>2<\/jats:sub>\n                    to form a \u03c0 complex\n                    <jats:bold>3<\/jats:bold>\n                    . DFT calculations reveal two significant interactions in\n                    <jats:bold>3<\/jats:bold>\n                    : the donation from the Bi\u2013Sn \u03c0\u2010bonding orbital to the 5s orbital of the Ag atom, and the backdonation from the 4d orbital of Ag to the Bi\u2013Sn \u03c0* orbital. These interactions conform to the Dewar\u2212Chatt\u2212Duncanson model for \u03c0\u2010complexes, highlighting the unique bonding characteristics of stannabismuthene.\n                  <\/jats:p>","DOI":"10.1002\/anie.3856989","type":"journal-article","created":{"date-parts":[[2026,7,6]],"date-time":"2026-07-06T14:20:42Z","timestamp":1783347642000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Isolation and Reactivity of a Stannabismuthene"],"prefix":"10.1002","volume":"65","author":[{"given":"Yifan","family":"Zhu","sequence":"first","affiliation":[{"name":"State Key Laboratory and Institute of Elemento\u2010Organic Chemistry, Frontiers Science Center for New Organic Matter, Academy for Advanced Interdisciplinary Studies, College of Chemistry Nankai University  Tianjin 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