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Herein, we present an efficient catalyst toward N\n                    <jats:sub>2<\/jats:sub>\n                    O decomposition containing short\u2010range ordered RhO\n                    <jats:italic>\n                      <jats:sub>x<\/jats:sub>\n                    <\/jats:italic>\n                    and CeO\n                    <jats:italic>\n                      <jats:sub>x<\/jats:sub>\n                    <\/jats:italic>\n                    species anchored to the Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    spinel. The activity enhancement relative to Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    is non\u2010additive with respect to the RhO\n                    <jats:italic>\n                      <jats:sub>x<\/jats:sub>\n                    <\/jats:italic>\n                    \/Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    and CeO\n                    <jats:italic>\n                      <jats:sub>x<\/jats:sub>\n                    <\/jats:italic>\n                    \/Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    interfaces and is uniquely linked to the modulation of the Co and Rh oxidation states at a synergistic Rh\u2013O\u2013Co\u2013O\u2013Ce interface. This ensemble provides increased redox flexibility and facilitated lattice oxygen activation, resulting in markedly enhanced N\n                    <jats:sub>2<\/jats:sub>\n                    O decomposition. Kinetic analysis and\n                    <jats:italic>operando<\/jats:italic>\n                    modulated excitation x\u2010ray absorption spectroscopy (ME\u2010XAS) provide direct mechanistic evidence that N\n                    <jats:sub>2<\/jats:sub>\n                    O decomposition proceeds via a multi\u2010site, cooperative Mars\u2010van Krevelen pathway, in which Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    \u2013CeO\n                    <jats:sub>2<\/jats:sub>\n                    acts as an oxygen reservoir enabling the redox cycling of RhO\n                    <jats:italic>\n                      <jats:sub>x<\/jats:sub>\n                    <\/jats:italic>\n                    species. This study highlights the ability of mixed metal oxide catalysts to exploit interfacial effects to achieve improved activity in redox\u2010mediated reactions and offers a rationale for the engineering of metal oxide\u2013metal oxide catalysts guided by\n                    <jats:italic>operando<\/jats:italic>\n                    spectroscopy.\n                  <\/jats:p>","DOI":"10.1002\/anie.7890563","type":"journal-article","created":{"date-parts":[[2026,6,23]],"date-time":"2026-06-23T07:41:15Z","timestamp":1782200475000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":2,"title":["Cooperative Redox Catalysis of N\n                    <sub>2<\/sub>\n                    O Decomposition by Short\u2010Range RhO\n                    <i>\n                      <sub>x<\/sub>\n                    <\/i>\n                    and CeO\n                    <i>\n                      <sub>x<\/sub>\n                    <\/i>\n                    Anchored to Co\n                    <sub>3<\/sub>\n                    O\n                    <sub>4<\/sub>"],"prefix":"10.1002","volume":"65","author":[{"ORCID":"https:\/\/orcid.org\/0009-0007-4257-3404","authenticated-orcid":false,"given":"Daniel C.","family":"Cano\u2010Blanco","sequence":"first","affiliation":[{"name":"PSI Center for Energy and Environmental Sciences Paul Scherrer Institute Villigen PSI Switzerland"},{"name":"Institute of Chemical Sciences and Engineering \u00c9cole polytechnique f\u00e9d\u00e9rale de Lausanne (EPFL) Lausanne Switzerland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-5948-8184","authenticated-orcid":false,"given":"Silvio","family":"Bellomi","sequence":"additional","affiliation":[{"name":"Institute of Materials Chemistry Technische Universit\u00e4t Wien  Vienna 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