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In this work, we synthesized an adaptive Pd\n                    <jats:sub>4<\/jats:sub>\n                    L\n                    <jats:sub>2<\/jats:sub>\n                    coordination cage using the newly developed pyridinium\u2010based ligand\n                    <jats:bold>L<\/jats:bold>\n                    with\n                    <jats:italic>cis<\/jats:italic>\n                    \u2010capped Pd (II) salt. Upon guest encapsulation, conformational adjustment provides direct structural evidence for the adaptive nature of cage\n                    <jats:bold>1<\/jats:bold>\n                    by X\u2010ray crystallographic study. Within the hydrophobic pocket of the capsule, 4\u2010(1\u2010hydroxy\u20101\u2010phenylethyl) phenol (\n                    <jats:bold>S1<\/jats:bold>\n                    ), a known\n                    <jats:italic>para<\/jats:italic>\n                    \u2010quinone methide (\n                    <jats:italic>p<\/jats:italic>\n                    \u2010QM) precursor, undergoes spontaneous dehydration to the alkene product\n                    <jats:bold>P1<\/jats:bold>\n                    in water. Kinetic studies and control experiments reveal that the cage\n                    <jats:bold>1<\/jats:bold>\n                    plays a vital role in significantly accelerating the dehydration process, affording the alkene product with markedly enhanced efficiency compared to the background reaction. Then generated alkene products act as a chemical stimulus driving the transformation of Pd\n                    <jats:sub>4<\/jats:sub>\n                    L\n                    <jats:sub>2<\/jats:sub>\n                    to a Pd\n                    <jats:sub>6<\/jats:sub>\n                    L\n                    <jats:sub>3<\/jats:sub>\n                    conjoined cage through an induced\u2010fit mechanism, as unambiguously confirmed by SCXRD. This work offers fresh insights into enzyme\u2010like adaptive behavior and unveils responsive supramolecular catalysis.\n                  <\/jats:p>","DOI":"10.1002\/anie.8746400","type":"journal-article","created":{"date-parts":[[2026,9,24]],"date-time":"2026-09-24T07:32:06Z","timestamp":1790235126000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Product\u2010Triggered Adaptive Evolution From a Pd\n                    <sub>4<\/sub>\n                    L\n                    <sub>2<\/sub>\n                    to a Pd\n                    <sub>6<\/sub>\n                    L\n                    <sub>3<\/sub>\n                    Conjoined Cage via Catalytic Dehydration of\n                    <i>p<\/i>\n                    \u2011Quinone Methide Precursors"],"prefix":"10.1002","author":[{"given":"Chen\u2010Chen","family":"Li","sequence":"first","affiliation":[{"name":"State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou P. 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