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Persistent organic pollutants (POPs), polycyclic aromatic hydrocarbons (PAHs) and microplastics are increasingly recognized as transboundary threats due to their long\u2010range atmospheric transport and accumulation. Despite international regulatory efforts, such as the Stockholm Convention and the EU's new air quality directives, data on deposition fluxes remain sparse and highly variable due to methodological inconsistencies and analytical limitations. Key challenges arise from the trace levels of target analytes, the complexity of environmental matrices and the absence of standardized sampling and analytical protocols. Overcoming these limitations is crucial for establishing robust monitoring systems and supporting evidence\u2010based risk assessments. This review highlights recent developments and methodological innovations in the study of bulk atmospheric deposition of organic pollutants. Key areas of focus include (1) a critical evaluation of sampling devices and strategies, with an emphasis on bottle\u2010funnel and passive sampler designs that influence data quality, (2) advances in extraction and sample preparation techniques, including liquid\u2013liquid and solid\u2010phase extraction tailored to trace\u2010level environmental contaminants, (3) identification of key analytical constraints and variability in recovery efficiencies across different compound classes and analytical workflows, (4) a synthesis of over 160 peer\u2010reviewed studies offering a comparative framework for future monitoring campaigns and harmonization of analytical approaches.<\/jats:p>","DOI":"10.1002\/ansa.70062","type":"journal-article","created":{"date-parts":[[2026,1,1]],"date-time":"2026-01-01T07:40:01Z","timestamp":1767253201000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Atmospheric Deposition of Organic Pollutants: A\u00a0Comprehensive Review of Sampling and Analytical Methodologies"],"prefix":"10.1002","volume":"7","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-6641-106X","authenticated-orcid":false,"given":"Iva","family":"Smoljo","sequence":"first","affiliation":[{"name":"Division of Environmental Hygiene Institute for Medical Research and Occupational Health  Zagreb Croatia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-2661-2465","authenticated-orcid":false,"given":"Gordana","family":"Menda\u0161","sequence":"additional","affiliation":[{"name":"Division of Environmental Hygiene Institute for Medical Research and Occupational Health  Zagreb Croatia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Gordana","family":"Pehnec","sequence":"additional","affiliation":[{"name":"Division of Environmental Hygiene Institute for Medical Research and Occupational Health  Zagreb Croatia"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2025,12,31]]},"reference":[{"key":"e_1_2_15_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.scitotenv.2020.139414"},{"key":"e_1_2_15_3_1","first-page":"707","article-title":"Concentrations of PAHs and Other Gaseous Pollutants in the Atmosphere of a Rural Area","volume":"51","author":"Jakovljevi\u0107 I.","year":"2016","journal-title":"Journal of Environmental Science and Health\u2014Part A Toxic\/Hazardous Substances and Environmental Engineering"},{"key":"e_1_2_15_4_1","doi-asserted-by":"publisher","DOI":"10.1007\/s11356-015-4777-z"},{"key":"e_1_2_15_5_1","doi-asserted-by":"publisher","DOI":"10.1007\/s00128-011-0516-4"},{"key":"e_1_2_15_6_1","unstructured":"EEA Air Quality in Europe\u20102020 Report. 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