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Carbon tetrachloride and ethylenediamine were used as the sources of carbon and nitrogen, respectively. The resulting MCN materials were characterized with low\u2010 and high\u2010angle powder XRD, nitrogen adsorption, high\u2010resolution (HR) SEM, HR\u2010TEM, elemental analysis, X\u2010ray photoelectron spectroscopy, and X\u2010ray absorption near\u2010edge structure techniques. The carbonization temperature plays a critical role in controlling not only the crystallinity, but also the nitrogen content and textural parameters of the samples, including specific surface area and specific pore volume. The nitrogen content of MCN decreases with a concomitant increase in specific surface area and specific pore volume, as well as the crystallinity of the samples, as the carbonization temperature is increased. The results also reveal that the structural order of the materials is retained, even after heat treatment at temperatures up to 900\u2009\u00b0C with a significant reduction of the nitrogen content, but the structure is partially damaged at 1000\u2009\u00b0C. The carbon dioxide adsorption capacity of these materials is not only dependent on the textural parameters, but also on the nitrogen content. The MCN prepared at 900\u2009\u00b0C, which has an optimum BET surface area and nitrogen content, registers a carbon dioxide adsorption capacity of 20.1\u2005mmol\u2009g<jats:sup>\u22121<\/jats:sup> at 273\u2005K and 30\u2005bar, which is much higher than that of mesoporous silica, MCN\u20101, activated carbon, and multiwalled carbon nanotubes.<\/jats:p>","DOI":"10.1002\/asia.201601707","type":"journal-article","created":{"date-parts":[[2017,1,16]],"date-time":"2017-01-16T22:23:08Z","timestamp":1484605388000},"page":"595-604","source":"Crossref","is-referenced-by-count":21,"title":["Effect of Heat Treatment on the Nitrogen Content and Its Role on the Carbon Dioxide Adsorption Capacity of Highly Ordered Mesoporous Carbon Nitride"],"prefix":"10.1002","volume":"12","author":[{"given":"Kripal S.","family":"Lakhi","sequence":"first","affiliation":[{"name":"Future Industries Institute Division of Information Technology, Engineering and Environment Mawson Lakes Campus University of South Australia  Adelaide 5095 Australia"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Dae\u2010Hwan","family":"Park","sequence":"additional","affiliation":[{"name":"Future Industries Institute Division of Information Technology, Engineering and Environment Mawson Lakes Campus University of South Australia  Adelaide 5095 Australia"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Stalin","family":"Joseph","sequence":"additional","affiliation":[{"name":"Future Industries Institute Division of Information Technology, Engineering and Environment Mawson Lakes Campus University of South Australia  Adelaide 5095 Australia"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Siddulu N.","family":"Talapaneni","sequence":"additional","affiliation":[{"name":"Future Industries Institute Division of Information Technology, Engineering and Environment Mawson Lakes Campus University of South Australia  Adelaide 5095 Australia"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Ugo","family":"Ravon","sequence":"additional","affiliation":[{"name":"SABIC Corporate Research and Development Center at KAUST Saudi Basic Industries Corporation  Thuwal 23955 Saudi Arabia"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Khalid","family":"Al\u2010Bahily","sequence":"additional","affiliation":[{"name":"SABIC Corporate Research and Development Center at KAUST Saudi Basic Industries Corporation  Thuwal 23955 Saudi Arabia"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Ajayan","family":"Vinu","sequence":"additional","affiliation":[{"name":"Future Industries Institute Division of Information Technology, Engineering and Environment Mawson Lakes Campus University of South Australia  Adelaide 5095 Australia"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2017,2,8]]},"reference":[{"key":"e_1_2_6_1_1","first-page":"1134","volume":"114","author":"Nandi M.","year":"2014","journal-title":"Chem. 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