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A new composite composed of Ru\u2010Pd nanoparticles supported on CFAC (Ru\u2010Pd@CFAC) has been prepared by microwave\u2010thermal reduction in the presence of the support. Characterization by XRD, Raman, BET, FE\u2010SEM\/TEM, FT\u2010IR, TGA, XPS, HAADF\u2010STEM\u2010EDS, H<jats:sub>2<\/jats:sub>\u2010chemisorption, H<jats:sub>2<\/jats:sub>\u2010TPR, and ICP\u2010AES was used to analyze the catalyst. This catalyst is found to be efficient for the reduction of hexavalent chromium (Cr<jats:sup>VI<\/jats:sup>), potassium ferricyanide (K<jats:sub>3<\/jats:sub>[Fe(CN)<jats:sub>6<\/jats:sub>]), 4\u2010nitrophenol (4\u2010NP), and pendimethalin (PDM), at room temperature, and remains stable, even after several repeated runs. 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