{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,29]],"date-time":"2026-10-29T18:38:48Z","timestamp":1793299128262,"version":"4.5.0"},"reference-count":144,"publisher":"Wiley","issue":"23","license":[{"start":{"date-parts":[[2020,10,28]],"date-time":"2020-10-28T00:00:00Z","timestamp":1603843200000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":["aces.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["Chemistry \u0097 An Asian Journal"],"published-print":{"date-parts":[[2020,12]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>Three new hetero\u2010metallic copper(II)\u2010manganese(II) complexes, [(CuL)<jats:sub>2<\/jats:sub>Mn<jats:sub>3<\/jats:sub>(C<jats:sub>6<\/jats:sub>H<jats:sub>5<\/jats:sub>CO<jats:sub>2<\/jats:sub>)<jats:sub>6<\/jats:sub>] (<jats:bold>1<\/jats:bold>), [(CuL)<jats:sub>2<\/jats:sub>Mn(CH<jats:sub>3<\/jats:sub>CO<jats:sub>2<\/jats:sub>)<jats:sub>2<\/jats:sub>] (<jats:bold>2<\/jats:bold>), and {[(CuL)<jats:sub>2<\/jats:sub>Mn(C<jats:sub>6<\/jats:sub>H<jats:sub>5<\/jats:sub>CH<jats:sub>2<\/jats:sub>CO<jats:sub>2<\/jats:sub>)<jats:sub>2<\/jats:sub>]\u2009\u22c5\u20092CH<jats:sub>3<\/jats:sub>CN} (<jats:bold>3<\/jats:bold>), have been synthesized using [CuL] as \u2018\u2018metalloligand\u2019\u2019 (where H<jats:sub>2<\/jats:sub>L=N,N\u2032\u2010bis(2\u2010hydroxynaphthyl\u2010methylidene)\u20101,3\u2010propanediamine). Single\u2010crystal structural analyses show an almost linear penta\u2010nuclear structure for complex <jats:bold>1<\/jats:bold> where a square planar [CuL] unit is connected to each of the two terminal Mn<jats:sup>II<\/jats:sup> ions of a linear, centrosymmetric [Mn<jats:sub>3<\/jats:sub>(benzoate)<jats:sub>6<\/jats:sub>] unit through the double phenoxido bridges. Both complexes <jats:bold>2<\/jats:bold> and <jats:bold>3<\/jats:bold> possess a linear tri\u2010nuclear structure where two terminal square\u2010pyramidal [CuL] units are bonded to the central Mn<jats:sup>II<\/jats:sup> ion through double phenoxido oxygen atoms along with a <jats:italic>syn\u2010syn<\/jats:italic> bridging acetate (for <jats:bold>2<\/jats:bold>)\/phenyl acetate (for <jats:bold>3<\/jats:bold>). All three complexes exhibit catecholase, and phenoxazinone synthase\u2010like activities under aerial conditions. For catecholase like activity, the turnover numbers (<jats:italic>k<\/jats:italic><jats:sub>cat<\/jats:sub>) are 595, 40, and 205\u2005h<jats:sup>\u22121<\/jats:sup> whereas, for phenoxazinone synthase like activity, the turnover numbers are 25, 4, and 11\u2005h<jats:sup>\u22121<\/jats:sup> for complexes <jats:bold>1\u20133<\/jats:bold>, respectively. The mechanism of both catalytic oxidase activities is proposed on the basis of mass spectral evidences. Variable\u2010temperature (2\u2013300\u2005K) dc molar magnetic susceptibility measurements of <jats:bold>1<\/jats:bold> reveal antiferromagnetic interactions between the Cu\u2212Mn centres (<jats:italic>J<\/jats:italic><jats:sub>1<\/jats:sub>=\u221229.3\u2005cm<jats:sup>\u22121<\/jats:sup>), and also between the Mn\u2212Mn centres of the [Mn<jats:sub>3<\/jats:sub>(benzoate)<jats:sub>6<\/jats:sub>] unit (<jats:italic>J<\/jats:italic><jats:sub>2<\/jats:sub>=\u22120.68\u2005cm<jats:sup>\u22121<\/jats:sup>). On increasing the magnetic field at 2\u2005K, its ground spin state changes from <jats:italic>S<\/jats:italic>=3\/2 to <jats:italic>S<\/jats:italic>=5\/2 at 4 T, attributable to the low value of <jats:italic>J<\/jats:italic><jats:sub>2<\/jats:sub> which makes the excited spin states close in energy with the ground spin state. Complexes <jats:bold>2<\/jats:bold> and <jats:bold>3<\/jats:bold> show antiferromagnetic coupling interactions between the Cu\u2212Mn pairs with <jats:italic>J<\/jats:italic> values of \u22129.51, and \u22125.32\u2005cm<jats:sup>\u22121<\/jats:sup>, respectively.<\/jats:p>","DOI":"10.1002\/asia.202000706","type":"journal-article","created":{"date-parts":[[2020,7,28]],"date-time":"2020-07-28T20:01:09Z","timestamp":1595966469000},"page":"4055-4069","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":27,"title":["Modulation of Nuclearity in Cu<sup>II<\/sup>\u2212Mn<sup>II<\/sup> Complexes of a N<sub>2<\/sub>O<sub>2<\/sub> Donor Ligand Depending upon Carboxylate Anions: Structures, Magnetic Properties and Catalytic Oxidase Activities"],"prefix":"10.1002","volume":"15","author":[{"given":"Sayantan","family":"Ganguly","sequence":"first","affiliation":[{"name":"Department of Chemistry University College of Science University of Calcutta  92, A. P. C. Road Kolkata 700 009 India"},{"name":"Department of Chemistry Taki Government College  Taki, Hasnabad West Bengal 743429 India"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"J\u00falia","family":"Mayans","sequence":"additional","affiliation":[{"name":"Instituto de Ciencia Molecular (ICMol) Universitat de Val\u00e8ncia  c\/ Catedr\u00e1tico Jos\u00e9 Beltr\u00e1n 2 46980 Paterna Val\u00e8ncia Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2026-7565","authenticated-orcid":false,"given":"Ashutosh","family":"Ghosh","sequence":"additional","affiliation":[{"name":"Department of Chemistry University College of Science University of Calcutta  92, A. P. C. 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