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Using a Co(II)\u2010catalyst [Co<jats:sup>II<\/jats:sup><jats:sub>2<\/jats:sub>(<jats:bold>L<jats:sup>a<\/jats:sup><\/jats:bold>)<jats:sub>2<\/jats:sub>Cl<jats:sub>2<\/jats:sub>] <jats:bold>(1\u2009a)<\/jats:bold> bearing redox\u2010active 2\u2010(phenyldiazenyl)\u20101,10\u2010phenanthroline) (<jats:bold>L<jats:sup>a<\/jats:sup><\/jats:bold>) scaffold, various substituted pyrroles and pyridines were synthesized in good yields, taking alcohol as one of the primary feedstock. Pyrroles were synthesized by the equimolar reaction of 2\u2010amino and secondary alcohols. A series of 2,4,6\u2010substituted symmetrical pyridines were prepared via a three\u2010component reaction of NH<jats:sub>4<\/jats:sub>OAc with 1\u2009:\u20092.2 molar primary and secondary alcohols, respectively. Unsymmetrically substituted 2,4,6\u2010trisubstituted, 2,4,5,6\u2010tetrasubstituted, and 2,3,4,5,6\u2010pentasubstituted pyridines were achieved via a multi\u2010component coupling reaction of alcohols and NH<jats:sub>4<\/jats:sub>OAc. Catalyst <jats:bold>1\u2009a<\/jats:bold> showed encouraging results during the gram\u2010scale synthesis of these <jats:italic>N<\/jats:italic>\u2010heterocycles. Mechanistic investigation revealed synergistic involvement of cobalt metal and the ligand during the catalytic reactions.<\/jats:p>","DOI":"10.1002\/asia.202401038","type":"journal-article","created":{"date-parts":[[2024,12,23]],"date-time":"2024-12-23T10:19:20Z","timestamp":1734949160000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Ligand Assisted Co(II)\u2010Catalyzed Multicomponent Synthesis of Substituted Pyrroles and Pyridines"],"prefix":"10.1002","volume":"20","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-7695-9902","authenticated-orcid":false,"given":"Subhajit","family":"Chakraborty","sequence":"first","affiliation":[{"name":"Department of Chemistry Indian Institute of Engineering Science and Technology Shibpur Botanic Garden  Howrah 711103 India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Arijit","family":"Singha Mohapatra","sequence":"additional","affiliation":[{"name":"Department of Chemistry Indian Institute of Engineering Science and Technology Shibpur Botanic Garden  Howrah 711103 India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Subhangi","family":"Saha","sequence":"additional","affiliation":[{"name":"Department of Chemistry Indian Institute of Engineering Science and Technology Shibpur Botanic Garden  Howrah 711103 India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Sutanuva","family":"Mandal","sequence":"additional","affiliation":[{"name":"Department of Chemistry Banwarilal Bhalotia College  Ushagram, Asansol, West Bengal India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8872-1413","authenticated-orcid":false,"given":"Nanda D.","family":"Paul","sequence":"additional","affiliation":[{"name":"Department of Chemistry Indian Institute of Engineering Science and Technology Shibpur Botanic Garden  Howrah 711103 India"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2025,1,10]]},"reference":[{"key":"e_1_2_8_1_1","unstructured":"\u00a0"},{"key":"e_1_2_8_2_2","volume-title":"Pharmaceutical Chemistry: Drug Synthesis, Vol.\u20051","author":"Roth H. 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