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The single\u2010crystal X\u2010ray analysis shows that the three studied compounds crystallize in the monoclinic <jats:italic>C<\/jats:italic>2\/<jats:italic>c<\/jats:italic>, <jats:italic>Pnma<\/jats:italic> orthorhombic and triclinic <jats:italic>P<\/jats:italic>\n space groups, with the two former compounds being polymorphs that are isostructural but differ in their symmetries. From the crystallographic results, a common packing arrangement is established, with C<jats:sub>60<\/jats:sub> and [Ni(Bz4TMTAA)] molecules organised around one\u2010dimensional hollow channels, associated 1\u2009:\u20091 and 1\u2009:\u20092 complexation of the macrocycle and the fullerene molecules, the latter being organised into hexagonal arrays. Interestingly, one of the structures showed a skewed hexagonal channel arrangement with the introduction of water molecules. Hirshfeld surface analyses have been used to investigate non\u2010covalent interactions and cumulative \u03c0\u2026\u03c0, C\u2212H\u2026\u03c0, H\u2026H, and N\u2026C<jats:sub>60<\/jats:sub> interactions between fullerene C<jats:sub>60<\/jats:sub> and [Ni(Bz<jats:sub>4<\/jats:sub>TMTAA)] host molecule which are deemed the stabilizing factors for forming the sophisticated arrangements in the solid\u2010state. differences.<\/jats:p>","DOI":"10.1002\/asia.202401363","type":"journal-article","created":{"date-parts":[[2025,1,27]],"date-time":"2025-01-27T03:49:06Z","timestamp":1737949746000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":2,"title":["Solid State Self\u2010Assembly of an Extended Curved\u2010Arm Nickel(II) Macrocycle with Fullerene 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