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In this work, we report a novel type of ORR electrocatalyst with Fe and Co sites anchored on N,P\u2010codoped hierarchically ordered macro\u2010\/mesoporous carbon (FeCo\/NP\u2010HOMMC) through a facile one\u2010pot, controllable synthesis method with the aid of dual\u2010templating technique. The FeCo\/NP\u2010HOMMC catalyst shows robust ORR performance under alkaline conditions with a half\u2010wave potential (\n                    <jats:italic>E<\/jats:italic>\n                    <jats:sub>1\/2<\/jats:sub>\n                    ) of 0.90\u2005V vs. reversible hydrogen electrode (RHE), significantly surpassing the commercial 20\u2005wt% Pt\/C catalyst, while also exhibiting remarkable long\u2010term stability and great methanol tolerance. Control experiments reveal that the superior performance of the FeCo\/NP\u2010HOMMC catalyst for ORR benefits from the synergistic catalysis of highly dispersed Fe and Co dual active sites, and the advantages of the unique hierarchically ordered macro\u2010\/mesoporous structure, which can provide improved active site accessibility, excellent conductivity, and maximized mass\/charge transport.\n                  <\/jats:p>","DOI":"10.1002\/asia.202401761","type":"journal-article","created":{"date-parts":[[2025,3,11]],"date-time":"2025-03-11T08:49:15Z","timestamp":1741682955000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Hierarchically Ordered Macro\u2010\/Mesoporous N,P\u2010Codoped Carbon with Fe\u2010Co Dual Sites for Efficient Electrocatalytic Oxygen Reduction"],"prefix":"10.1002","volume":"20","author":[{"given":"Fulin","family":"Li","sequence":"first","affiliation":[{"name":"State Key Laboratory of Organic\u2212Inorganic Composites Beijing University of Chemical Technology  Beijing 100029 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jing","family":"Dong","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Organic\u2212Inorganic Composites Beijing University of Chemical Technology  Beijing 100029 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tingting","family":"Sun","sequence":"additional","affiliation":[{"name":"Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials School of Chemistry and Biological Engineering University of Science and Technology Beijing  Beijing 100083 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Pianpian","family":"Zhang","sequence":"additional","affiliation":[{"name":"Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials School of Chemistry and Biological Engineering University of Science and Technology Beijing  Beijing 100083 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yixin","family":"Zhang","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Organic\u2212Inorganic Composites Beijing University of Chemical Technology  Beijing 100029 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Anvar A.","family":"Zakhidov","sequence":"additional","affiliation":[{"name":"The Alan G. MacDiarmid NanoTech Institute University of Texas at Dallas  Richardson Texas 75083 United States"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ray H.","family":"Baughman","sequence":"additional","affiliation":[{"name":"The Alan G. 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