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In this study, a series of Bi<jats:sub>2<\/jats:sub>Ti<jats:sub>2<\/jats:sub>O<jats:sub>7<\/jats:sub>\/BaTiO<jats:sub>3<\/jats:sub> heterojunctions were synthesized via hydrothermal method, demonstrating superior photocatalytic NO removal efficiency (94%) compared to individual components. Comprehensive characterizations confirmed the formation of a tightly coupled heterojunction with enhanced visible\u2010light absorption and charge separation. Optical and electrochemical analyses revealed that the composite facilitates efficient electron\u2010hole separation (supported by reduced PL intensity and lower charge\u2010transfer resistance in EIS) while retaining strong redox potentials, consistent with an S\u2010scheme charge\u2010transfer mechanism. Additionally, the increased surface area (BET) and porosity further promote reactant adsorption. Trapping experiments and electron paramagnetic resonance (EPR) confirmed that e\u207b, h\u207a, and \u00b7O<jats:sub>2<\/jats:sub>\u207b are key reactive species. The synergistic effects of improved charge dynamics, optimized light utilization, and interfacial electron transfer collectively contribute to the enhanced photocatalytic performance.<\/jats:p>","DOI":"10.1002\/asia.202500651","type":"journal-article","created":{"date-parts":[[2025,6,13]],"date-time":"2025-06-13T10:06:51Z","timestamp":1749809211000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Construction of a Novel Solar\u2010Light\u2010Driven Bismuth Titanate\/Barium Titanate Photocatalyst for Significantly Enhanced Purification of Nitric Oxide"],"prefix":"10.1002","volume":"20","author":[{"given":"Wei","family":"Zhao","sequence":"first","affiliation":[{"name":"School of Energy &amp; Power Engineering Jiangsu University  Zhenjiang 212013 P. R. 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