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Over the past decade, significant advances have been made in developing catalytic strategies that enable precise control over phosphorus stereochemistry, expanding both the structural diversity and synthetic utility of these scaffolds. This review highlights recent progress in two key areas: direct P\u2013C bond formation and desymmetrization. P\u2013C bond\u2010forming approaches include cross\u2010coupling reactions of secondary phosphines or their oxides with aryl, alkyl, or benzyl halides, as well as hydrophosphination of alkenes and alkynes. Desymmetrization strategies encompass nucleophilic substitution at P(V) centers, cyclization, C\u2013H activation (CHA), phenolic \u2013OH activation, and P\u2013O alkylation\/arylation. Mechanistic insights into these transformations have been discussed, along with the derivatization of P\u2010chiral products and their applications in catalysis, L design, and bioactive molecule synthesis. This comprehensive overview shall serve as a valuable resource for researchers working in asymmetric organophosphorus chemistry.<\/jats:p>","DOI":"10.1002\/asia.202500952","type":"journal-article","created":{"date-parts":[[2025,12,16]],"date-time":"2025-12-16T04:12:49Z","timestamp":1765858369000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":8,"title":["P\u2010Chiral Organophosphorus Compounds: Synthesis, Mechanism, and Applications"],"prefix":"10.1002","volume":"21","author":[{"given":"Amol C.","family":"Chandanshive","sequence":"first","affiliation":[{"name":"Polymer Science and Engineering Division CSIR\u2010National Chemical Laboratory  Pune India"},{"name":"Academy of Scientific and Innovative Research (AcSIR)  Ghaziabad India"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8442-1480","authenticated-orcid":false,"given":"Samir 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