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This bimetallic Fe^Fe^Co complex was explored in an alkene oxidation reaction to give aldehydes as products, which could be accomplished via water oxidation catalysis at room temperature. In the proposed mechanism, both metal\u2010ligand cooperativity as well as bimetallic participation of the two metals Co and Fe (of one unit of ferrocene moiety) further facilitates the two oxidation cycles altogether. The peroxo intermediate in the catalytic water oxidation cycle is proposed to be the crucial intermediate species for the conversion of the unsaturated system into its corresponding aldehydes.<\/jats:p>","DOI":"10.1002\/asia.71009","type":"journal-article","created":{"date-parts":[[2026,10,7]],"date-time":"2026-10-07T08:13:17Z","timestamp":1791360797000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Redox Active Cobalt NHC Catalyst for Oxidation of Alkenes to Carbonyl Compounds at Room Temperature: Water as Source of Oxygen"],"prefix":"10.1002","volume":"21","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-2988-8758","authenticated-orcid":false,"given":"Debashree","family":"Bora","sequence":"first","affiliation":[{"name":"Materials Sciences Group, Coal, Energy &amp; Materials Sciences Division (CEMSD) CSIR\u2010North East Institute of Science and Technology  Jorhat Assam India"},{"name":"Academy of Scientific 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