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The possible mechanism of the CL reaction was described using UV\u2013Vis. absorption and CL spectra. Experimental variables were optimized by applying a univariate approach, and a linear calibration curve was obtained in the range of 1.0\u2009\u00d7\u200910<jats:sup>\u22123<\/jats:sup>\u20132.0\u00a0mg\u2009L<jats:sup>\u22121<\/jats:sup> (<jats:italic>R<\/jats:italic><jats:sup>2<\/jats:sup>\u2009=\u20090.9994, <jats:italic>n<\/jats:italic>\u2009=\u20099) with a limit of detection of 5.0\u2009\u00d7\u200910<jats:sup>\u22124<\/jats:sup>\u00a0mg\u2009L<jats:sup>\u22121<\/jats:sup> (S\/N\u2009=\u20093) and an injection throughput of 200\u2009h<jats:sup>\u22121<\/jats:sup>. This approach was successfully applied to determine THI in fresh water by using solid\u2010phase extraction and achieved a good recovery rate of 94%\u2013110% with a relative standard deviation of 1.9%\u20133.7% (<jats:italic>n<\/jats:italic>\u2009=\u20094). The results obtained were compared with the reported FI\u2010CL and high\u2010performance liquid chromatography\u2013ultraviolet methods, and the three methods did not differ significantly at the 95% confidence limit.<\/jats:p>","DOI":"10.1002\/bio.4389","type":"journal-article","created":{"date-parts":[[2022,9,23]],"date-time":"2022-09-23T21:03:05Z","timestamp":1663966985000},"page":"2041-2049","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":14,"title":["Determination of thiram residues in fresh water using flow injection diperiodatonickelate(IV)\u2013quinine chemiluminescence detection"],"prefix":"10.1002","volume":"37","author":[{"ORCID":"https:\/\/orcid.org\/0000-0003-3865-1565","authenticated-orcid":false,"given":"Muhammad","family":"Asghar","sequence":"first","affiliation":[{"name":"Department of Chemistry University of Balochistan  Quetta Pakistan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mohammad","family":"Yaqoob","sequence":"additional","affiliation":[{"name":"Department of Chemistry University of Balochistan  Quetta Pakistan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Nusrat","family":"Munawar","sequence":"additional","affiliation":[{"name":"Department of Chemistry Sardar Bahadur Khan Women University  Quetta Pakistan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Abdul","family":"Nabi","sequence":"additional","affiliation":[{"name":"Department of Chemistry University of Balochistan  Quetta Pakistan"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2022,10,12]]},"reference":[{"issue":"164","key":"e_1_2_7_2_1","first-page":"209","volume":"26","author":"Barley S.","year":"1976","journal-title":"J. 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