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The aggregation\u2010induced emission (AIE) properties of compounds <jats:bold>1<\/jats:bold>\u2013<jats:bold>3<\/jats:bold> were tested in different water fraction (<jats:italic>f<\/jats:italic><jats:sub>w<\/jats:sub>) of tetrahydrofuran (THF). The pyrrolo[3,2\u2010b]pyrrole derivative <jats:bold>3<\/jats:bold> containing TPE units exhibited typical AIE features with an enhanced emission (\u223c32\u2010fold) in the solid state <jats:italic>versus<\/jats:italic> in solution; compounds <jats:bold>1<\/jats:bold> and <jats:bold>2<\/jats:bold> exhibited an aggregation\u2010caused quenching effect. In addition, the steric and electronic effects of the peripheral moieties on the emission behavior, both in solution and in the solid state, have been investigated. Moreover, pyrrolo[3,2\u2010b]pyrrole <jats:bold>1<\/jats:bold> exhibits high sensitivity and selectivity for dichloromethane and chloroform solvents, with the system displaying a new emission peak and fast response time under ultraviolet irradiation.<\/jats:p>","DOI":"10.1002\/bio.4640","type":"journal-article","created":{"date-parts":[[2023,12,6]],"date-time":"2023-12-06T00:00:01Z","timestamp":1701820801000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["New pyrrolo[3,2\u2010b]pyrroles with AIE characteristics for detection of dichloromethane and chloroform"],"prefix":"10.1002","volume":"39","author":[{"given":"Shuning","family":"Yu","sequence":"first","affiliation":[{"name":"Guangdong Provincial Key Laboratory of Functional Soft Condensed Matter, School of Material and Energy Guangdong University of Technology  Guangzhou P. R. 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