{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,10,30]],"date-time":"2025-10-30T22:21:04Z","timestamp":1761862864495,"version":"build-2065373602"},"reference-count":26,"publisher":"Wiley","issue":"4","license":[{"start":{"date-parts":[[2009,8,2]],"date-time":"2009-08-02T00:00:00Z","timestamp":1249171200000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Biomedical Chromatography"],"published-print":{"date-parts":[[2010,4]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>A GC\u2010MS procedure for simultaneously determining and validating kresoxim\u2010methyl and boscalid has been developed in fruit, vegetable and soil matrices. The method was based on one\u2010step liquid\u2013liquid extraction with acetone and dichloromethane solvents. Estimated limits of detection (LODs) for kresoxim\u2010methyl and boscalid were 0.006 and 0.015\u2009mg\/kg, and limits of quantification (LOQs) were 0.02 and 0.05\u2009mg\/kg, respectively. The intra\u2010 and inter\u2010 precision were achieved with RSD better than 13.8 and 14.5%, and recoveries were in the range of 77.1\u201398.7% for kresoxim\u2010methyl and 72.8\u2013105.1% for boscalid. The expanded uncertainties calculated at 0.1\u2009mg\/kg were below 18%. Concentration levels for residues of the two fungicides in melon samples from field trials collected 7 days after the last application were clearly below the established MRL values. Copyright \u00a9 2009 John Wiley &amp; Sons, Ltd.<\/jats:p>","DOI":"10.1002\/bmc.1301","type":"journal-article","created":{"date-parts":[[2009,8,2]],"date-time":"2009-08-02T21:58:06Z","timestamp":1249250286000},"page":"367-373","source":"Crossref","is-referenced-by-count":10,"title":["Residue analysis of kresoxim\u2010methyl and boscalid in fruits, vegetables and soil using liquid\u2013liquid extraction and gas chromatography\u2013mass 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