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Iron composite nanoparticles were prepared using green technology. CE was carried out using a silica capillary (60 cm \u00d7 50 \u03bcm i.d.), phosphate buffer (50 m<jats:sc>m<\/jats:sc>, 8.0 pH)\u2013acetonitrile (95:5, v\/v) as the background electrolyte, 10 kV voltage, 280 nm detection, 20 s injection time and 27 \u00b1 1\u00b0C temperature. Frusemide was used as an internal standard. The values of migration time, electrophoretic mobility, electrophoretic velocity and theoretical plates of chloramphenicol were 12.254 min, 4.44 \u00d7 10, 7.41 \u00d7 10 and 11,227. The limits of detection and quantitation of chloramphenicol were 0.1 and 1.0 \u03bcg\/mL. Recovery of chloramphenicol in the standard solution was 95%. Solid\u2010phase membrane micro\u2010tip extraction and capillary electrophoresis methods may be used to analyze chloramphenicol in human plasma and urine samples of any patient.<\/jats:p>","DOI":"10.1002\/bmc.3769","type":"journal-article","created":{"date-parts":[[2016,5,26]],"date-time":"2016-05-26T09:52:20Z","timestamp":1464256340000},"page":"1935-1941","source":"Crossref","is-referenced-by-count":26,"title":["Determination of chloramphenicol in biological matrices by solid\u2010phase membrane micro\u2010tip extraction and capillary electrophoresis"],"prefix":"10.1002","volume":"30","author":[{"given":"Afzal","family":"Hussain","sequence":"first","affiliation":[{"name":"Department of Pharmacognosy College of Pharmacy, King Saud University  P.O. Box 2457 Riyadh 11451 Kingdom of Saudi Arabia"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Mohammed F.","family":"Alajmi","sequence":"additional","affiliation":[{"name":"Department of Pharmacognosy College of Pharmacy, King Saud University  P.O. Box 2457 Riyadh 11451 Kingdom of Saudi Arabia"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Imran","family":"Ali","sequence":"additional","affiliation":[{"name":"Department of Chemistry Jamia Millia Islamia (Central University)  New Delhi 110025 India"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2016,6,27]]},"reference":[{"key":"e_1_2_8_2_1","doi-asserted-by":"publisher","DOI":"10.1201\/9780203911112"},{"key":"e_1_2_8_3_1","doi-asserted-by":"publisher","DOI":"10.1002\/bmc.593"},{"key":"e_1_2_8_4_1","first-page":"14","article-title":"Nano\u2010hyphenation technologies","author":"Ali I.","year":"2009","journal-title":"Laboratory Plus International"},{"key":"e_1_2_8_5_1","doi-asserted-by":"publisher","DOI":"10.1002\/0470867825"},{"key":"e_1_2_8_6_1","doi-asserted-by":"publisher","DOI":"10.1201\/9781420019407"},{"key":"e_1_2_8_7_1","doi-asserted-by":"publisher","DOI":"10.1002\/jssc.200800123"},{"key":"e_1_2_8_8_1","volume-title":"Nano Chromatography and Capillary Electrophoresis: Pharmaceutical and Environmental Analyses","author":"Ali I.","year":"2009"},{"key":"e_1_2_8_9_1","doi-asserted-by":"publisher","DOI":"10.1039\/c1ay05496a"},{"key":"e_1_2_8_10_1","first-page":"18","article-title":"Fast analysis of third\u2010generation cephalosporins in human plasma by SPE and HPLC methods","author":"Ali I.","year":"2011","journal-title":"LC\u2010GC The Magazine of Separation Science"},{"key":"e_1_2_8_11_1","doi-asserted-by":"publisher","DOI":"10.1039\/c3ay40276b"},{"key":"e_1_2_8_12_1","doi-asserted-by":"publisher","DOI":"10.1007\/s13762-015-0919-6"},{"key":"e_1_2_8_13_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.molliq.2016.02.088"},{"key":"e_1_2_8_14_1","doi-asserted-by":"publisher","DOI":"10.1080\/10826076.2016.1152583"},{"key":"e_1_2_8_15_1","doi-asserted-by":"publisher","DOI":"10.1080\/09540109409354853"},{"key":"e_1_2_8_16_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0378-4347(00)00049-9"},{"key":"e_1_2_8_17_1","volume-title":"Kinetic aspect of analytical Chemistry","author":"Mottola H.A.","year":"1988"},{"key":"e_1_2_8_18_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0003-2670(99)00314-1"},{"key":"e_1_2_8_19_1","doi-asserted-by":"publisher","DOI":"10.1002\/elps.200800188"}],"container-title":["Biomedical Chromatography"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.wiley.com\/onlinelibrary\/tdm\/v1\/articles\/10.1002%2Fbmc.3769","content-type":"application\/pdf","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/api.wiley.com\/onlinelibrary\/tdm\/v1\/articles\/10.1002%2Fbmc.3769","content-type":"unspecified","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/analyticalsciencejournals.onlinelibrary.wiley.com\/doi\/pdf\/10.1002\/bmc.3769","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2025,10,9]],"date-time":"2025-10-09T19:05:19Z","timestamp":1760036719000},"score":1,"resource":{"primary":{"URL":"https:\/\/analyticalsciencejournals.onlinelibrary.wiley.com\/doi\/10.1002\/bmc.3769"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2016,6,27]]},"references-count":18,"journal-issue":{"issue":"12","published-print":{"date-parts":[[2016,12]]}},"alternative-id":["10.1002\/bmc.3769"],"URL":"https:\/\/doi.org\/10.1002\/bmc.3769","archive":["Portico"],"relation":{},"ISSN":["0269-3879","1099-0801"],"issn-type":[{"value":"0269-3879","type":"print"},{"value":"1099-0801","type":"electronic"}],"subject":[],"published":{"date-parts":[[2016,6,27]]}}}