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The process parameters (amount of raw material, immersion time and washing time) were analyzed to optimize the process by means of Box\u2010Behnken design via response surface methodology. The optimum conditions were achieved by ~10\u2005g fresh lemon peel, and ~15\u2005min immersion time and ~13\u2005min washing time. The difference between the actual (89.37\u2005mg\/g limonene) and predicted (90.85\u2005mg\/g limonene) results was satisfactory (&lt;2\u2009%). \u03b1\u2010Terpinene, \u03b2\u2010pinene, citral, \u0263\u2010terpinene and linalool were determined as other major volatiles in the peel extract. FT\u2010IR and<jats:sup>1<\/jats:sup>H\u2010 and<jats:sup>13<\/jats:sup>C\u2010NMR spectroscopies were applied to verify the identified volatile compounds.<\/jats:p>","DOI":"10.1002\/cbdv.202300767","type":"journal-article","created":{"date-parts":[[2023,7,10]],"date-time":"2023-07-10T02:09:45Z","timestamp":1688954985000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Development of an Optimized Method to Obtain a Limonene\u2010Rich Concentrate from the Discarded Lemon Peels"],"prefix":"10.1002","volume":"20","author":[{"given":"Ferhan","family":"Balci\u2010Torun","sequence":"first","affiliation":[{"name":"Akdeniz University Faculty of Tourism Department of Gastronomy and Culinary Art 07058 Antalya Turkey"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"\u0130rem","family":"Toprak\u00e7\u0131","sequence":"additional","affiliation":[{"name":"Istanbul University-Cerrahpa\u015fa Faculty of Engineering Chemical Engineering Department Avcilar 34320 Istanbul Turkey"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Nahide Gul\u015fah","family":"Deniz","sequence":"additional","affiliation":[{"name":"Istanbul University-Cerrahpa\u015fa Faculty of Engineering Chemistry Department Division of Organic Chemistry Avcilar 34320 Istanbul Turkey"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Sinem","family":"Ortaboy","sequence":"additional","affiliation":[{"name":"Istanbul University-Cerrahpa\u015fa Faculty of Engineering Chemistry Department, Division of Physical Chemistry Avcilar 34320 Istanbul Turkey"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Mehmet","family":"Torun","sequence":"additional","affiliation":[{"name":"Akdeniz University Faculty of Engineering, Food Engineering Department 07058 Antalya Turkey"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9989-9823","authenticated-orcid":false,"given":"Selin","family":"\u015eahin","sequence":"additional","affiliation":[{"name":"Istanbul University-Cerrahpa\u015fa Faculty of Engineering Chemical Engineering Department Avcilar 34320 Istanbul Turkey"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2023,8,8]]},"reference":[{"key":"e_1_2_9_1_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.wasman.2014.06.026"},{"key":"e_1_2_9_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.biortech.2016.05.006"},{"key":"e_1_2_9_3_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.bej.2019.107298"},{"key":"e_1_2_9_4_1","doi-asserted-by":"crossref","first-page":"387","DOI":"10.3390\/catal11030387","volume":"11","author":"Satira A.","year":"2021","journal-title":"Catal."},{"key":"e_1_2_9_5_1","doi-asserted-by":"publisher","DOI":"10.22207\/JPAM.15.3.01"},{"key":"e_1_2_9_6_1","doi-asserted-by":"crossref","DOI":"10.1016\/j.heliyon.2020.e05703","volume":"7","author":"Nagoor Meeran M. 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