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[R<jats:sup>Fc<\/jats:sup>SnCl<jats:sub>3<\/jats:sub>\u22c5HCl] (<jats:bold>C<\/jats:bold>; R<jats:sup>Fc<\/jats:sup>\u00a0=\u00a0CMe<jats:sub>2<\/jats:sub>CH<jats:sub>2<\/jats:sub>C(Me)\uf8feN\uf8ffN\uf8feC(Me)Fc) and [SnCl<jats:sub>6<\/jats:sub>]<jats:sup>2\u2212<\/jats:sup> formed {(R<jats:sup>Fc<\/jats:sup>SnCl<jats:sub>2<\/jats:sub>)<jats:sub>3<\/jats:sub>[Sn(OH)<jats:sub>6<\/jats:sub>]}[SnCl<jats:sub>3<\/jats:sub>] (<jats:bold>3\u2009a<\/jats:bold>) and {(R<jats:sup>Fc<\/jats:sup>SnCl<jats:sub>2<\/jats:sub>)<jats:sub>3<\/jats:sub>[Sn(OH)<jats:sub>6<\/jats:sub>]}[PhSeO<jats:sub>3<\/jats:sub>] (<jats:bold>3\u2009b<\/jats:bold>), bearing an unprecedented [Sn<jats:sub>4<\/jats:sub>O<jats:sub>6<\/jats:sub>] unit, in a one\u2010pot synthesis or stepwise through [(R<jats:sup>Fc<\/jats:sup>SnCl<jats:sub>2<\/jats:sub>)<jats:sub>2<\/jats:sub>Se] (<jats:bold>1<\/jats:bold>) plus [(R<jats:sup>Fc<\/jats:sup>SnCl<jats:sub>2<\/jats:sub>)SePh] (<jats:bold>2<\/jats:bold>). 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