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Herein, a cluster\u2010cooperative assemble strategy is developed to synthesize Ti CPs. By utilizing various bifunctional ligands containing carboxylate acids and N\u2010donor groups, we successfully assembled the zero\u2010dimensional (0D) [(Ti<jats:sub>3<\/jats:sub>O)(<jats:italic>i<\/jats:italic>PrO)<jats:sub>8<\/jats:sub>]<jats:sup>2+<\/jats:sup> or [(Ti<jats:sub>4<\/jats:sub>O<jats:sub>2<\/jats:sub>)(<jats:italic>i<\/jats:italic>PrO)<jats:sub>6<\/jats:sub>]<jats:sup>6+<\/jats:sup> clusters into one\u2010dimensional (1D) tube\u2010, ribbon\u2010, or helical chain\u2010shape architectures, two\u2010dimensional (2D) layered structures, and a rare parallel 2D\u2192three\u2010dimensional (3D) polycatenation framework with various copper iodide dopants, including rhombus\u2010 or wing\u2010shaped Cu<jats:sub>2<\/jats:sub>I<jats:sub>2<\/jats:sub> and tetrahedron\u2010 or ladder\u2010shaped Cu<jats:sub>4<\/jats:sub>I<jats:sub>4<\/jats:sub>. The as\u2010synthesized compounds display strong absorption in the visible region with narrow band gaps ranging from 1.70 to 2.72\u2005eV and exhibit good photocatalytic activities in the degradation of organic pollutants.<\/jats:p>","DOI":"10.1002\/chem.201705013","type":"journal-article","created":{"date-parts":[[2017,12,18]],"date-time":"2017-12-18T23:22:39Z","timestamp":1513639359000},"page":"2952-2961","source":"Crossref","is-referenced-by-count":46,"title":["Designed Cluster Assembly of Multidimensional Titanium Coordination Polymers: Syntheses, Crystal Structure and Properties"],"prefix":"10.1002","volume":"24","author":[{"given":"Chao","family":"Wang","sequence":"first","affiliation":[{"name":"State Key Laboratory of Rare Earth Resource Utilization Changchun Institute of Applied Chemistry Chinese Academy of Sciences  Changchun Jilin 130022 China"},{"name":"University of Chinese Academy of Sciences  Beijing 100049 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